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D8 discover vario

Manufactured by Bruker

The D8 Discover Vario is a flexible X-ray diffractometer (XRD) from Bruker. It is designed for a wide range of applications in materials science and nanotechnology research.

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3 protocols using d8 discover vario

1

Powder XRD Analysis of Perovskites

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Powder XRD patterns
of mechanosynthesized layered and 3D perovskites were recorded with
a Bruker D8 Discover Vario diffractometer with a Cu Kα1 monochromator (1.5406 Å) from 2θ = 2–50°.
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2

Comprehensive Characterization of M/CeO2 Catalysts

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Powder X-ray diffraction (PXRD) of all M/CeO2 catalysts was measured from 2θ = 20–80° on a Bruker D8 Discover Vario diffractometer by using Cu Kɑ (L = 1.54 Å) radiation that was operated at 40 kV and 40 mA. X-ray photoelectron spectroscopy (XPS) measurements were carried out on an Axis Supra (Kratos Analytical) using the monochromated Ka X-ray line of an Aluminium anode. The pass energy was set to 40 eV with a step size of 0.15 eV. The samples were electrically insulated from the sample holder and an electron flood gun was used to neutralise the charges. The binding energy scale was then referenced at 284.8 eV using the aliphatic line of the C1s orbital. Inductively coupled plasma mass spectrometry (ICP-MS) was performed on a Perkin Elmer NexIon 350 spectrometer for elemental analysis. Scanning transmission electron microscopy (STEM) images for Rh/CeO2, Pd/CeO2 and Ir/CeO2 were captured on a FEI Tecnai Osiris electron microscope at 200 KeV, while high resolution (HR) STEM images for Ru/CeO2 and Pt/CeO2 were captured on a FEI Titan Themis electron microscope at 300 keV. High-angle annular dark field (HAADF) imaging mode was used for all STEM imaging. Energy-dispersive X-ray spectroscopy (EDX) was performed at 20 KeV.
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3

Powder XRD Characterization of Perovskites

Check if the same lab product or an alternative is used in the 5 most similar protocols
Powder XRD patterns of mechanosynthesized
layered and 3D perovskites were recorded with a Bruker D8 Discover
Vario diffractometer with a Cu Kα1 monochromator
(1.5406 Å) from 2θ = 5–50°.
+ Open protocol
+ Expand

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