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Ultima 4 x ray diffraction

Manufactured by Rigaku
Sourced in Japan

The Ultima IV X-ray diffraction system is a versatile analytical instrument designed for materials characterization. It utilizes X-ray diffraction techniques to provide structural and compositional information about a wide range of solid materials. The Ultima IV is capable of performing various X-ray diffraction measurements, including phase identification, lattice parameter determination, and texture analysis.

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3 protocols using ultima 4 x ray diffraction

1

Structural Characterization of Materials

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Scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FTIR) spectroscopy were used to examine the morphology, crystal phase, and nature of the surface molecular groups of the materials, respectively. X-ray diffraction (XRD, Rigaku – Ultima IV X-ray diffraction, scan speed 4.00=min, scan range 3–90) was used to investigate crystallinity and was performed using monochromatic Cu K radiation and a positional sensitive detector. FTIR spectra were recorded using KBr transparent discs at 64 scans between 4000 and 400 cm−1 with a resolution of 4 cm−1. The 105 N vacuumed-dried samples were pressed into a transparent disk with a diameter of 14 mm by applying force. The absorbance of KBr-sample discs was measured.
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2

Characterization of GO/g-C3N4/ZnO Composite

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The GO/g-C3N4/ZnO structure was examined using a Rigaku Ultima IV X-ray diffraction
(XRD). Versa PobeII X-ray photoelectron spectroscopy (XPS) was used
to investigate the surface characteristics and chemical composition.
Surface morphology was examined using a scanning electron microscope
(JEOL, JSM7600-F). The absorption spectra for the degradation of methylene
blue (MB) were obtained through a spectrophotometer (DR 6000, Hach
Lang).
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3

Comprehensive Physicochemical Characterization of Composites

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The crystal phase of composites was studied by Rigaku Ultima IV X-ray diffraction (Rigaku, Japan). The surface morphologies were characterized by scanning electron microscope (FEI Quanta 650, Netherlands). Fourier transform infrared spectroscopy (FTIR, 4000–600 cm−1) was recorded on Thermo Scientific Nicolet 10 (Thermo, USA) using ATR model. X-ray photoelectron spectroscopy (XPS) was performed with a Thermo Scientific K-Alpha X-ray photoelectron spectrometer (Thermo, USA) using mono AlKa radiation (hv=1486.6 eV) to investigate elemental compositions of composites. Thermogravimetric analysis (TGA) was carried out for composites under nitrogen atmosphere by using a Discovery TGA 5500 instruments (TA, USA) with a heating rate of 5.0 °C min−1 from 30 °C to 790 °C. SHA-B constant temperature water bath oscillator (Suzhou NINENBO Technology Co., Ltd.). DZF-6032 vacuum drying ovens (Shanghai yiheng scientific instrument co., Ltd.). MC-3020 laser engraving machine was used for cutting filter paper (Shandong mingchuang laser equipment co., Ltd.).
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