T butyldimethylsilanol
Manufactured by Merck Group
T-butyldimethylsilanol is a silyl protecting group used in organic synthesis. It is a colorless liquid with a boiling point of approximately 160°C. The compound is commonly used to protect alcohol functional groups during multi-step chemical reactions.
Automatically generated - may contain errors
2 protocols using t butyldimethylsilanol
1
Synthesis and Characterization of Antibacterial Polymers
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dl -lactide and glycolide were obtained from Beijing CONAN Polymer R&D Center (Beijing, People’s Republic of China). BA, stannous 2-ethylhexanoate, t-butyldimethylsilanol, triphenylsilanol, N,N′-carbonyldiimidazole (CDI), and Triton X-100 were purchased from Sigma-Aldrich (Shanghai, People’s Republic of China). Mueller–Hinton broth (MHB) powder, Mueller–Hinton (MH) agar, Salmonella Shigella agar, MacConkey agar, and Edwards Medium (Modified) were purchased from AoBoX (Beijing, People’s Republic of China) and were used to prepare bacterial broths according to the manufacturer’s instructions. All the other regents and chemicals were of analytical or chromatographic grade and were purchased from Concord Technology (Tianjing, People’s Republic of China).
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2
Organosilicon Standards for oVMS Analysis
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Six commercially available organosilicon
standards were used as oVMS surrogates for method development: trimethylsilanol
(97.5%, Sigma-Aldrich), 1-trimethylsilylmethanol (95%, Thermo Scientific),
tris(tert-pentoxy)silanol (99.99%, Sigma-Aldrich),
tris(tert-butoxy)silanol (99.999%, Sigma-Aldrich),
dimethylphenylsilanol (95%, Sigma-Aldrich), and t-butyldimethylsilanol (99%, Sigma-Aldrich). Acetonitrile was purchased
from Fisher Scientific (Optima) and ultrapure water (18.2 MW resistivity)
was generated by a water purification system on site (Thermo, Barnsted
EasyPure-II). Ammonia (20-22% as NH3, Fisher Scientific)
and ammonium bicarbonate (99.0%, Sigma-Aldrich) were used to prepare
the buffer added to mobile phases to improve ionization.
standards were used as oVMS surrogates for method development: trimethylsilanol
(97.5%, Sigma-Aldrich), 1-trimethylsilylmethanol (95%, Thermo Scientific),
tris(tert-pentoxy)silanol (99.99%, Sigma-Aldrich),
tris(tert-butoxy)silanol (99.999%, Sigma-Aldrich),
dimethylphenylsilanol (95%, Sigma-Aldrich), and t-butyldimethylsilanol (99%, Sigma-Aldrich). Acetonitrile was purchased
from Fisher Scientific (Optima) and ultrapure water (18.2 MW resistivity)
was generated by a water purification system on site (Thermo, Barnsted
EasyPure-II). Ammonia (20-22% as NH3, Fisher Scientific)
and ammonium bicarbonate (99.0%, Sigma-Aldrich) were used to prepare
the buffer added to mobile phases to improve ionization.
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