The vesicle morphology of the Lip-DT was characterized with a HR-SEM (Thermo scientific Apreo S) operating at 15.00 kV and HR-TEM (JEOL-JEM-2100 Plus) operating at 200 kV. For HR-SEM analysis 20 μL of the Lip-DT was drop casted on a clean glass coverslip and dried at RT. For HR-TEM analysis a 10 μL drop of a Lip-DT was placed on a 200-mesh copper grid and covered by carbon-stabilized Formvar® film. After 1 min, excess fluid was removed from the grid. The morphology and fluorescent nature of the vesicles were visualized using a Leica DM6 Fluorescent Microscope with Cryostat. Dynamic light scattering analysis (Zetasizernano ZS, Malvern Instruments, Malvern, U.K.) was carried out to find the size distribution and surface charge of the Lip-DT and PCDA/DMPC-based liposomes. Dynamic light scattering (DLS) measurements were performed using the samples diluted to approximately 0.05 mM.17 (link)
Apreo s
Manufactured by JEOL
Sourced in Japan
The Apreo S is a field-emission scanning electron microscope (FE-SEM) designed for high-resolution imaging and analysis of a wide range of samples. It utilizes a stable cold-field emission electron gun to provide a high-brightness, small-diameter electron beam for high-resolution imaging. The Apreo S offers advanced capabilities for materials characterization, nanotechnology research, and other applications requiring detailed surface analysis at the nanometer scale.
Automatically generated - may contain errors
Lab products found in correlation
Jem 2100 plus, by JEOL (4 mentions)
Irtracer 100, by Shimadzu (3 mentions)
D8 advance, by Bruker (2 mentions)
Zetasizer nano z, by Malvern Panalytical (1 mentions)
Uv3600 spectrometer uv drs, by Horiba (1 mentions)
Jsm 2100plus, by JEOL (1 mentions)
Uv 3600, by Shimadzu (1 mentions)
Nexsa base, by Thermo Fisher Scientific (1 mentions)
Apreo s, by Thermo Fisher Scientific (1 mentions)
5 protocols using apreo s
1
Characterizing Lip-DT Vesicle Morphology
2
Characterization of Photocatalyst Nanoparticles
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Powder X-ray diffraction analysis of the synthesized photocatalysts was analysed through BRUKER USA D8 Advance, Davinci powder X-ray diffractometer. The surface nature of the nanoparticles was examined by FESEM (Thermoscientific Apreo S) and HRTEM (JEOL, JSM-2100plus) microscopes. The optical behaviour was studied by a Shimadzu UV3600+ spectrometer (UV-DRS) and HORIBA Fluorolog (PL). The surface elements confirmation of the nanoparticles was carried out by PHI Versaprobe III. The FTIR spectrum of the synthesized nanoparticles were examined using a SHIMADZU, IRTRACER-100 with KBr mode.
3
Comprehensive Characterization of Zinc Oxide Nanoparticles
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The green synthesized ZnO NPs and ZnO–Ag NPs have undergone a wide range of characterizations to understand their morphology, surface chemistry, size, etc. Using the aqueous medium, the absorption spectra were recorded at 200–800 nm using a UV-vis spectrophotometer (Shimadzu UV-3600, Japan). Fourier transform infrared spectrophotometry (SHIMADZU, Japan, IRTRACER 100) was used to analyze the surface chemistry and functionality of the metal oxide nanoparticles. The spectrum was recorded in the wavenumber range of 4000–400 cm−1. The crystalline nature of the ZnO and ZnO–Ag NPs was recorded using an X-ray diffractometer (BRUKER D8 Advance, USA), and scans were performed from (2θ) 10° to 90° at a rate of 5° min−1. The dynamic light scattering method was utilized to determine the hydrodynamic particle size and zeta potential (Malvern/Nano ZS-90, UK). Elemental analysis was determined from the XPS spectrum (PHI5000, USA). High-resolution SEM was carried out for the morphological evaluation of synthesized nanoparticles performed with Thermosceintific Apreo S, Scanning Electron Microscope. And the high-resolution TEM (JEOL Japan, JEM-2100 Plus transmission electron microscope). The elemental confirmation was evaluated using an EDAX (energy dispersive X-ray analyzer) equipped with the HRTEM.
4
Comprehensive Characterization of Materials
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Using Bruker USA D8 Advances,
the crystallographic studies were done. A brief study on morphological
features was analyzed using high-resolution scanning electron microscopy
(HRSEM) (Thermo Scientific Apreo S) and high-resolution transmission
electron microscopy (HRTEM) (JEOL Japan, JEM-2100 Plus). The nitrogen
adsorption–desorption isotherms were performed with a Quantachrome-ASiQwin
(version 5.0) apparatus and the porosity measurement was evaluated
by Brunauer–Emmett–Teller (BET) and Barret–Joyner–Halenda
(BJH) methods. With the aid of X-ray photoelectron spectroscopy (XPS)
(Thermo Fisher Scientific Nexsa base), the elemental composition and
metallic states were confirmed and electrochemical characterizations
were implemented with an OrigaLys eletro-flex electrochemical workstation.
the crystallographic studies were done. A brief study on morphological
features was analyzed using high-resolution scanning electron microscopy
(HRSEM) (Thermo Scientific Apreo S) and high-resolution transmission
electron microscopy (HRTEM) (JEOL Japan, JEM-2100 Plus). The nitrogen
adsorption–desorption isotherms were performed with a Quantachrome-ASiQwin
(version 5.0) apparatus and the porosity measurement was evaluated
by Brunauer–Emmett–Teller (BET) and Barret–Joyner–Halenda
(BJH) methods. With the aid of X-ray photoelectron spectroscopy (XPS)
(Thermo Fisher Scientific Nexsa base), the elemental composition and
metallic states were confirmed and electrochemical characterizations
were implemented with an OrigaLys eletro-flex electrochemical workstation.
5
Advanced Techniques for Hybrid Material Characterization
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High-resolution scanning electron microscopy (HR-SEM, Thermoscientific Apreo S) and transmission electron microscopy (TEM, JEM-2100 Plus, JEOL) were utilized to predict the morphological, surface properties, and chemical content, and the selected area electron diffraction (SAED) pattern of produced h-BN, and PTh/h-BN hybrid. Energy dispersive spectroscopy (EDS-JEM-2100 Plus, JEOL, and Thermoscientific Apreo S) was utilized for elemental and chemical composition. The crystalline nature of the synthesized compound was examined by using X-ray diffraction spectroscopy (XRD system-X'pert powder, with Cu-Kα radiation (λ = 0.154 nm) Malvern Panalytical, United Kingdom) at 45 kV (tension) and 40 mA (current) with 0.02° per step scan and 1° per min speed. The functional groups of the synthesized materials were analyzed by Fourier Transform Infrared Spectroscopy (FT-IR) technique, (FT-IR spectrophotometer, Shimadzu, IR Tracer 100). The cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), differential pulse voltammetry (DPV), and amperometry (i–t curve) studies were carried out using CHI electrochemical workstation (CHI 760E, USA). All the measurements were performed at room temperature using a three-electrode setup. The counter, reference, and working electrodes were platinum wire (Pt), Ag/AgCl (3 M KCl), and glassy carbon electrode (GCE), respectively.
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