Triphenylphosphine

Manufactured by Nacalai Tesque

Triphenylphosphine is a colorless, crystalline solid organic compound with the formula PPh3. It is a common reagent used in organic synthesis and is widely employed in various laboratory applications.

Automatically generated - may contain errors

Lab products found in correlation

Mgcl2, by Nacalai Tesque (1 mentions) Rh2 oac 4, by Merck Group (1 mentions) Cu acac 2, by Merck Group (1 mentions) 1 hexanol, by Fujifilm (1 mentions) 1 dodecanol, by Nacalai Tesque (1 mentions) Copper chloride dihydrate, by Nacalai Tesque (1 mentions) Acetone, by Merck Group (1 mentions) Oleylamine, by Merck Group (1 mentions) Ethyl alcohol, by Merck Group (1 mentions)

2 protocols using triphenylphosphine

Synthesis of Diazoacetates and Reagents

Check if the same lab product or an alternative is used in the 5 most similar protocols

Tetrahydrofuran
(THF) and toluene were dried
over a Na/K alloy and Na, respectively, and distilled before use.
CH₂Cl₂ was dried over CaH₂ and used
without further purification. Cu(acac)₂ (TCI; >97%),
Rh₂(OAc)₄ (AZmax; 99%), RuCl(cod)Cp* (Sigma-Aldrich),
Grubbs first catalyst (Sigma-Aldrich; 97%), 1-hexanol (TCI; >98.0%),
diisopropyl azodicarboxylate (Wako; >90%), triphenylphosphine (Nacalai;
>98.0%), MgCl₂ (Nacalai; >97.0%), 1,8-diazabicyclo[5,4,0]-7-undecene
(DBU) (Nacalai; >97.0%), and 1-dodecanol (TCI; >99.0%) were
used as
received without further purification. Tosyl azide,²⁷ 4,4′-biphenylenediacetic acid,^{28 (link)} 1,4-phenylenediacetic acid,^{28 (link),29 (link)} and 2,2′-(9,9-dioctyl-9H-fluorene-2,7-diyl)diacetonitrile^{30 (link)} were prepared following the procedures reported in the literatures.
Methyl 2-diazo-2-phenylacetate^{17 (link)} was prepared
using tosyl azide as a diazo transfer agent following a reported general
procedure for this type of diazoketones. Caution! Extra care must
be taken for the preparation and handling of the diazoacetates because
of their potential explosiveness.

Shimomoto H., Moriya T.A., Mori T., Itoh T., Kanehashi S., Ogino K, & Ihara E. (2020). Single-Component Polycondensation of Bis(alkoxycarbonyldiazomethyl)aromatic Compounds To Afford Poly(arylene vinylene)s with an Alkoxycarbonyl Group on Each Vinylene Carbon Atom. ACS Omega, 5(10), 4787-4797.

+ Open protocol

+ Expand

Synthesis of Copper-Palladium Catalysts

Check if the same lab product or an alternative is used in the 5 most similar protocols

Palladium (II) bis(acetylacetonate) (Pd(acac)₂), 99%), Oleylamine (70%), ethyl alcohol (99.9%), and acetone (99.9%) were purchased from Sigma Aldrich. Copper chloride dihydrate (CuCl₂·2H₂O, 99%), triphenylphosphine (TPP, 99%), and commercial P25 (99.9% grade) were obtained from Nacalai Tesque, Acros Organics, and Degussa, respectively. The gases deployed in this research, such as high purity nitrogen (N₂, 99.999%), carbon dioxide (CO₂, 99.5%), and helium (He, 99.99%), were procured from Yusheng gas company, Taipei, Taiwan.

Elavarasan M., Yang W., Velmurugan S., Chen J.N., Yang T.C, & Yokoi T. (2022). Highly Efficient Photothermal Reduction of CO2 on Pd2Cu Dispersed TiO2 Photocatalyst and Operando DRIFT Spectroscopic Analysis of Reactive Intermediates. Nanomaterials, 12(3), 332.

+ Open protocol

+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!