Sb 2 s 3

Manufactured by Merck Group

Sourced in Japan

Sb₂S₃ is an inorganic compound with the chemical formula Sb₂S₃. It is a solid material that can be used as a laboratory reagent and in various industrial applications.

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Lab products found in correlation

4 protocols using sb 2 s 3

Synthesis and Characterization of Multicomponent Oxide Minerals

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Samples were synthesised from stoichiometric amounts of Fe 2 O 3 , Fe metal, MgO, Sb 2 O 3 and Sb 2 S 3 (all >99%, Aldrich), ground and heated within sealed quartz ampoules between 520 °C and 600 °C for between 48 hours and 1 month, with intermediate grinding. Slow cooling was necessary in order to minimise structural disorder. Phase purity was checked with laboratory X-ray powder diffraction (XRPD) equipment (Bruker D2 [Co Kα] and Bruker D8 [Cu Kα 1 ], both with PSD LynxEye dectector). Neutron powder diffraction (NPD) data were collected at Institut Laue-Langevin (D2B diffractometer, λ = 1.594 Å), Paul-Scherrer Institute (HRPT instrument, λ = 1.494 Å and 1.886 Å) and the ISIS facility, UK (GEM diffractometer, TOF) at a range of temperatures in He cryostats. Refinements were performed using GSAS with the EXPGUI interface. 9,10 Mineralogical samples were obtained from Systematic Mineralogy and removed from parent dolomite samples using a mineral drill. XRPD showed a small amount of residual dolomite within the samples.
Magnetic susceptibility measurements were obtained using a Quantum Design MPMS under field-cooled (FC) and zero-fieldcooled (ZFC) conditions, with an applied magnetic field of 500 Oe. Powdered sample was loaded into a gelatin capsule, and sample movement was suppressed using a small amount of PTFE tape. No diamagnetic correction was applied to the data.

Cumby J., Bayliss R.D., Berry F.J, & Greaves C. (2016). Synthetic analogues of Fe(ii)-Fe(iii) minerals containing a pentagonal 'Cairo' magnetic lattice. Dalton transactions (Cambridge, England : 2003), 45(29).

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Colloidal Nanocrystal Synthesis Protocols

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Selenium dioxide (SeO₂, 99.9+%,
Strem), oleic acid (OA, 90%, Aldrich), 1-octadecene (ODE, 90%, Aldrich),
methanol (Aldrich, 98%), cadmium nitrate tetrahydrate (Cd(NO₃)₂ × 4H₂O, 99.99%, Aldrich), CdO (99.99+,
Sigma-Aldrich), myristic acid (MA, 99%, Aldrich), sodium hydroxide
(NaOH, Aldrich), hexane (>95% Sigma-Aldrich), ethanol (99.8%, Fluka),
toluene (99%, Fischer), formamide (FA, 99.5+%, Aldrich), acetonitrile
(MeCN, 99.9%, Sigma-Aldrich), N-methyl formamide
(MFA, 99%, Aldrich), dimethylformamide (DMF, 99.8%, Sigma-Aldrich),
hydrazine (98%, anhydrous, Aldrich), potassium sulfide (K₂S, 99.5%, Strem), ammonium sulfide (40–48% solution in water,
Aldrich), antimony(III) sulfide (Sb₂S₃, 99.995%,
Aldrich), germanium(II) sulfide (GeS, 99.99%, Aldrich), sulfur (99.998%,
Sigma-Aldrich), As₂S₅ (99.99%, Sigma-Aldrich),
triethyloxonium tetrafluoroborate (98%, Fluka), Na₂S nanohydrate
(98%, Aldrich), ammonium thiocyanate (97.5%, Aldrich), sodium stannate
trihydrate (95%, Sigma-Aldrich), C₆D₆ (99.9%,
CIL), and DMSO-d₆ (99.9%, CIL) were used
as received.

Protesescu L., Nachtegaal M., Voznyy O., Borovinskaya O., Rossini A.J., Emsley L., Copéret C., Günther D., Sargent E.H, & Kovalenko M.V. (2015). Atomistic Description of Thiostannate-Capped CdSe Nanocrystals: Retention of Four-Coordinate SnS4 Motif and Preservation of Cd-Rich Stoichiometry. Journal of the American Chemical Society, 137(5), 1862-1874.

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Fabrication of Sodium-Ion Battery Anode

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Carbon black (Super C65, TIMCAL), carboxymethyl cellulose (CMC, Grade: 2200, Lot No. B1118282, Daicel Fine Chem Ltd.), NaClO₄ (98%, Alfa Aesar, additionally dried), propylene carbonate (BASF, battery grade), 4-fluoro-1,3-dioxolan-2-one (FEC, Hisunny Chemical, battery grade), 1 M solution of LiPF₆ in ethylene carbonate/dimethyl carbonate (EC/DMC, Novolyte, Celgard separator (Celgard 2400, 25 µm microporous monolayer polypropylene membrane, Celgard Inc. USA), glass microfiber separator (GF/D, Cat No. 1823–257, Whatman), Al foil (MTI Corporation), Na foil (Sigma-Aldrich), Li foil (MTI Corp.), Sb₂S₃ (99.995%, Sigma Aldrich), Coin-type cells (Hohsen Corp., Japan),

Kravchyk K.V., Kovalenko M.V, & Bodnarchuk M.I. (2020). Colloidal Antimony Sulfide Nanoparticles as a High-Performance Anode Material for Li-ion and Na-ion Batteries. Scientific Reports, 10, 2554.

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Synthesis and Characterization of Sb₂S₃ Materials

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Two different types of Sb₂S₃ samples were evaluated in this study: (1) Bulk crystalline Sb₂S₃ was obtained from Sigma Aldrich and used as it is (denoted as “Sb₂S₃” in the paper). (2) Crystalline Sb₂S₃ wire were made by an aqueous precipitation between SbCl₃ in acetone and sodium thiosulfate (Na₂S₂O₃) followed by a hydrothermal annealing at 150°C for 4 hours, adopted from procedure of Li et al.31 .
Structure of the materials was studied by powder X-ray diffraction (XRD) with a Cu K_alpha (Bruker). Morphology and particle size of the tested materials were studied by field emission scanning electron microscope (SEM) with a JOEL JSM-7600F.

Yu D.Y., Hoster H.E, & Batabyal S.K. (2014). Bulk antimony sulfide with excellent cycle stability as next-generation anode for lithium-ion batteries. Scientific Reports, 4, 4562.

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