1H, 13C, and 19F NMR spectra were acquired on Varian Mercury 400, VNMRS-500, and VNMRS-600 spectrometers and processed using MestReNova 12.0.1. All chemical shifts are reported in ppm and referenced to the residual 1H or 13C solvent peaks. Following abbreviations are used: (s) singlet, (bs s) broad singlet, (d) doublet, (t) triplet, (dd) doublet of doublets, etc. NMR spectra of all metal complexes were taken in 8” J. Young tubes (Wilmad or Norell) with Teflon valve plugs. MALDI-MS spectra were acquired on Bruker Autoflex Speed MALDI Mass Spectrometer. X-ray crystallography data were obtained on a Bruker APEX DUO single-crystal diffractometer equipped with an APEX2 CCD detector, Mo fine-focus and Cu micro-focus X-ray sources. IR spectra were obtained using Jasco FT/IR-4600 FT-IR Spectrometer.
Ft ir 4600 ft ir spectrometer
The FT/IR-4600 FT-IR Spectrometer is a Fourier Transform Infrared (FT-IR) spectroscopy instrument. It is designed to analyze the infrared absorption and emission characteristics of various materials. The device utilizes an interferometer to generate and detect infrared radiation, providing information about the molecular composition and structure of the sample under analysis.
Lab products found in correlation
4 protocols using ft ir 4600 ft ir spectrometer
Iridium-Catalyzed C-H Sulfonation of Heterocycles
Micro FT-IR Spectroscopy of Samples
micro FT-IR spectroscopy was performed using an IRT-7100 IR microscope
with the FT/IR-4600 FT-IR spectrometer (JASCO) equipped with a high
brilliant ceramic light source, liquid nitrogen-cooled single mid-band
MCT detector, and 32× Cassegrain objective (NA = 0.75). FT-IR
spectra were recorded in transmission mode as the average of 256 scans
from 600 to 4000 cm–1 at a spectral resolution of
4 cm–1, with an aperture size of 10 × 10 μm2. The measurement points were scanned at 2.5 × 2.5 and
10 × 10 μm2, and the spectra were converted
to text data files using Spectra Manager version 2 (JASCO).
Characterization of Organometallic Complexes
Synthesis and Characterization of Magnetic Nanoparticles
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