Lipase N435 derived from Candida antarctica (CAL-B) immobilized on acrylic resin (Sigma-Aldrich, St. Louis, MO, USA) was dried over P2O5 for 24 h prior to use. N,N-dimethylformamide (anhydrous, 99.8%), acetonitrile (anhydrous, 99.8%), tetrahydrofuran (anhydrous, 99.9%), xylitol (99%) and d -sorbitol (98%), stearoyl chloride (90%) and triethylamine were purchased from Sigma-Aldrich. Divinyl adipate (96%) was purchased from TCI GmbH (Eschborn, Germany). All chemicals were used without further purification. All other chemicals used in various stages like, diethyl ether, n-hexane, methanol and dichloromethane were purchased from Carl Roth (Karlsruhe, Germany).
Acrylic resin
Manufactured by Merck Group
Sourced in United States
Acrylic resin is a synthetic polymer material commonly used in laboratory equipment. It is a transparent, rigid, and shatter-resistant material that can be molded into various shapes and forms. Acrylic resin is known for its durability, chemical resistance, and optical clarity, making it suitable for a range of laboratory applications.
Automatically generated - may contain errors
Lab products found in correlation
Stearoyl chloride, by Merck Group (1 mentions)
Diethyl ether, by Carl Roth (1 mentions)
D sorbitol, by Merck Group (1 mentions)
N hexane, by Carl Roth (1 mentions)
Acetonitrile, by Merck Group (1 mentions)
Triethylamine, by Merck Group (1 mentions)
Tetrahydrofuran, by Merck Group (1 mentions)
Xylitol, by Merck Group (1 mentions)
N n dimethylformamide (dmf), by Merck Group (1 mentions)
Methanol, by Carl Roth (1 mentions)
Dichloromethane, by Carl Roth (1 mentions)
2 protocols using acrylic resin
1
Enzymatic Esterification of Polyols
2
Enzymatic Synthesis of Glycerol-Coated Silica
Check if the same lab product or an alternative is used in the 5 most similar protocols
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Approximately 30mg of silica gel was added to 25mg of glycerol, and it was then vortexed such that the silica was entirely coated with glycerol until the admixture was free flowing. Between 5–10mg of this material was added to a solution of the free acid (0.15mg) in 0.5ml diethyl ether containing 20mg of Candida antarctica lipase on acrylic resin (Sigma-Aldrich), and it was vortexed briefly. The reaction was left for 3 days, then the mixture was filtered and evaporated under nitrogen. The residue was reconstituted in ethanol and analyzed by LC-MS. Results for each compound reacted under these conditions are shown in Fig. 10 .
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