1 chloropentane

Manufactured by Merck Group

1-chloropentane is a chemical compound that is a clear, colorless liquid. It has the molecular formula C5H11Cl. 1-chloropentane is commonly used as a laboratory reagent and an intermediate in organic synthesis.

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3 protocols using 1 chloropentane

Synthesis of Colloidal Nanocrystal Superlattices

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Benzene (99.8%, anhydrous), n-butanol (99.8%,
anhydrous), 1-chloropentane (99%), cyclohexyl isocyanide
(98%), diphenylphosphine (98%), hexane (mixture of isomers, ≥99%,
anhydrous), isopropanol (99.5%, anhydrous), lead acetate trihydrate
(≥99.99%), methanol (99.8%, anhydrous), 1-octadecene (90%),
octane (≥99%, anhydrous), oleic acid (90%), pyrrolidine (≥99%),
selenium powder (99.99%, −100 mesh), tetrachloroethylene (≥99%,
anhydrous), toluene (99.8%, anhydrous), triethylamine (≥99%),
trifluoroacetic acid (99%), trifluoroacetic anhydride (≥99%),
trimethylbenzene (98%), and trioctylphosphine (90%) were purchased
from Sigma-Aldrich and used without further purification. Lead (II)
oxide (99.999+%) was purchased from Strem Chemicals. 1,4-Butanediol
(BD, 99%, ReagentPlus), di ethylene glycol (DEG, 99%), diphenyl ether
(≥99%), ethylene glycol (EG, 99.8%, anhydrous), and hexadecane
(≥99%) were purchased from Sigma-Aldrich and degassed under
vacuum for ∼14 h at 60 °C prior use. For superlattice
formation, a distillation of the EG did not result in a significant
difference in the quality of the formed superlattice (see Figure S1).

van der Sluijs M.M., Sanders D., Jansen K.J., Soligno G., Vanmaekelbergh D, & Peters J.L. (2022). On the Formation of Honeycomb Superlattices from PbSe Quantum Dots: The Role of Solvent-Mediated Repulsion and Facet-to-Facet Attraction in NC Self-Assembly and Alignment. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 126(2), 986-996.

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Synthesis and Characterization of Ionic Liquids

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1-butylimidazole (98%, Sigma-Aldrich), 1-chloropentane (99%, Sigma-Aldrich), potassium trifluoromethanesulfonate (KOTf, Sigma-Aldrich), sodium tetrafluoroborate (NaBF₄, Sigma-Aldrich), benzyl chloride (99%, Sigma-Aldrich), dimethyl sulfoxide-D₆ (DMSO‑d₆, 99.9%) + 0.05% V/V tetramethylsilane (TMS, Cambridge Isotope Laboratories, Inc.), NH₃ (99.99%), Ar gas (99.99%), and ethyl acetate (99.5%, Sigma-Aldrich) (Table 1) were used as received without any purification.Table 1

Materials for IL synthesis and characterization.

Table 1

Materials	Molecular formula	CAS Number	Purity	Company
1-butylimidazole	C₇H₁₂N₂	4316-42-1	98%	Sigma-Aldrich
1-chloropentane	C₅H₁₁Cl	543-59-9	99%
Potassium trifluoromethanesulfonate	CF₃KO₃S	2926-27-4	98%
Sodium tetrafluoroborate	NaBF₄	13755-29-8	98%
ethyl acetate	C₄H₈O₂	141-78-6	99.5%
Dimethyl sulfoxide-D₆+0.05% V/V tetramethylsilane	C₂H₆OS + Si(CH₃)₄	2206-27-1	99.9%	Cambridge Isotope Laboratories, Inc.
Ammonia	NH₃	–	99.9%	–
Argon	Ar	–	99.9%	–

Salman M., Lee J.W., Lee S.H., Lee M.H., Pham V.D., Kim M.S., Cho D, & Lee H.J. (2024). A comparative study of ammonia solubility in imidazolium-based ionic liquids with different structural compositions. Heliyon, 10(2), e24305.

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Thin Film Preparation with Anti-Octadecaborane Derivatives

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Thin films were prepared from the following polymers and anti-octadecaborane(22) and its derivatives. Polystyrene with molecular weight 350 000 g/mol (PS350; M_w ~ 350,000, M_n ~ 170,000) and 35,000 g/mol (PS35; M_w ~ 35,000), poly(N-ethyl-2-vinylcarbazole) (PVK; M_w ~ 990,000), and poly [2-methoxy-5-(2-ethylhexyloxy)-1,4-phenylenevinylene] (MEH-PPV; M_n 40,000–70,000) were purchased from Sigma Aldrich. A high-molecular-weight polymer poly [1-phenyl-2-[p-(trimethylsilyl)diphenyl]acetylene] (PTMSDPA, M_w ~ 10⁶) was prepared at the Faculty of Science of the Charles University in Prague according to the procedure described in [35 (link)]. Poly(dimethylsilane-methylphenylsilane) (PDMSi-MPSi; M_w ~ 82,000, M_n ~ 18,000) was obtained from Fluorochem Ltd., and polycarbonate Makrolon (PC, M_w ~ 58,000, M_n ~ 25,000) was obtained from Bayer. Octadecaborane anti-B₁₈H₂₂ (B, M = 216.58 g/mol) and its tetra-alkylated derivatives 3,3′,4,4′-Et₄-anti-B₁₈H₁₈ (BEt, M = 328.66 g/mol) and 3,3′,4,4′-Me₄-anti-B₁₈H₁₈ (BMe; M = 272.62 g/mol) were synthesized at the Institute of Inorganic Chemistry of the AS CR [25 (link)].
Our 1-chloropentane (99%), toluene (p.a.), and cyclohexane anhydrous (99.5%) stock was purchased from Sigma-Aldrich. Chloroform (stabilized with 2-methyl-2-butene, 99.8%) was obtained from Avantor. All these solvents were used for the preparation of solutions for spin coating.

Capkova T., Hanulikova B., Sevcik J., Urbanek P., Antos J., Urbanek M, & Kuritka I. (2022). Incorporation of the New anti-Octadecaborane Laser Dyes into Thin Polymer Films: A Temperature-Dependent Photoluminescence and Infrared Spectroscopy Study. International Journal of Molecular Sciences, 23(15), 8832.

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