The X-ray powder diffraction (XRPD) studies were carried by using a powder X-ray diffractometer (Rigaku Geigerflex XRD, Co., Japan). XRPD studies were measured at 40 kV and 45 mA. During XRPD studies the range of 2θ angle was used between 5° and 40° at a scan rate and step size of 5°/min and 0.01° respectively.7 (link)
Geigerflex xrd
Manufactured by Rigaku
Sourced in Japan
The Geigerflex XRD is a versatile X-ray diffractometer designed for laboratory use. It is capable of performing accurate phase identification and characterization of crystalline materials. The Geigerflex XRD utilizes a Geiger-Müller counter to detect the diffracted X-rays, providing reliable and reproducible data.
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Lab products found in correlation
3 protocols using geigerflex xrd
1
X-ray Powder Diffraction Analysis
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The X-ray powder diffraction (XRPD) studies were carried by using a powder X-ray diffractometer (Rigaku Geigerflex XRD, Co., Japan). XRPD studies were measured at 40 kV and 45 mA. During XRPD studies the range of 2θ angle was used between 5° and 40° at a scan rate and step size of 5°/min and 0.01° respectively.7 (link)
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The X-ray powder diffraction (XRPD) studies were carried by using a powder X-ray diffractometer (Rigaku Geigerflex XRD, Co., Japan). XRPD studies were measured at 40 kV and 45 mA. During XRPD studies the range of 2θ angle was used between 5° and 40° at a scan rate and step size of 5°/min and 0.01° respectively.7 (link)
2
Comprehensive Characterization of Drug-Loaded Nanoparticles
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Transmission electron microscopy (TEM) (Tecnai G2F30, USA) and scanning electron microscopy (SEM) (JEOL JSM-7001F) were used to identify the morphological and structural characteristics of SPS and ACHN. Differential scanning calorimetry (DSC) (DSC-60, Shimadzu, Japan) and X-ray diffraction patterns (XRD) (Rigaku Geigerflex XRD, Co., Japan) were used to characterize the physical properties of PTX and DOX within DOX-PTX-ACHN. Fourier transform infrared spectroscopy (FT-IR) (Bruker IFS 55, Switzerland) was used to determine whether PTX, DOX, and ACHN had an interaction.
3
Structural Analysis of 3DOMG and PMMA Nanospheres
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The structure and morphology of 3DOMG and PMMA nanospheres were examined by SEM (JEOL JSM-7001F, operated at 20 kV). The drug crystallinity was examined using a differential scanning calorimeter (DSC) (DSC-60, Shimadzu, Japan) at a constant heating rate of 10 C/min from 50 C to 300 C under a constant nitrogen flow of 150 mL/min. A powder X-ray diffractometer (PXRD) (Rigaku Geigerflex XRD, Company, Japan, Cu-Ka radiation, 30 kV and 30 mA Philips) was used to further investigate the physical state of FNB in 3DOMG. The step size was 0.02 , the scanning rate was 4 /min, and the range (2q) was from 3 to 60 . Fourier transform infrared (FTIR) spectra were recorded using an FT-IR spectrometer over the range 400-4000 cm À1 (Bruker IFS 55, Switzerland) and the KBr pellet technique.
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