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Dimethylsulfoxide

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Dimethylsulfoxide is a colorless, odorless, and water-soluble liquid. It is commonly used as a solvent in various laboratory applications.

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Lab products found in correlation

Ascorbic acid, by Bio-Rad (3 mentions) β cyclodextrin, by Bio-Rad (2 mentions) Bio gel p 10 medium, by Bio-Rad (2 mentions) Sodium hydroxide (naoh), by Merck Group (2 mentions) Sodium azide, by Merck Group (2 mentions) Diisopropyl ether, by Merck Group (1 mentions) Potassium carbonate, by Bio-Rad (1 mentions) Dichloromethane ch2cl2, by Merck Group (1 mentions) Acetone ch3coch3, by Merck Group (1 mentions) Copper sulfate pentahydrate, by Merck Group (1 mentions) Methanol, by Merck Group (1 mentions) Potassium iodide, by Merck Group (1 mentions) Dichloromethane, by Merck Group (1 mentions) Acetic acid, by Bio-Rad (1 mentions) Hydrochloric acid (hcl), by Bio-Rad (1 mentions) Potassium persulfate, by Merck Group (1 mentions) Ethanol, by Bio-Rad (1 mentions) Folin ciocalteu s phenol reagent, by Merck Group (1 mentions) Gallic acid, by Merck Group (1 mentions) Sodium carbonate, by Merck Group (1 mentions)

3 protocols using dimethylsulfoxide

1

Synthesis and Functionalization of Cyclotriphosphazenes

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All starting materials were commercially available reagent grade and were used without any further purification. Hexachlorocyclotriphosphazene (P3N3Cl6), 5-chloro-1-pentyne, 6-iodo-1-hexyne, hydroquinone, β-cyclodextrin (βCD), p-toluenesulfonyl chloride (Cl-Ts), p-toluenesulfonic acid (OH-Ts), N,N-dimethylformamide anhydrous (DMF), potassium carbonate (K2CO3), cesium carbonate (Cs2CO3), dimethylsulfoxide (DMSO), ascorbic acid (H2Asc), Bio-Gel P-10 medium from Bio-Rad (Hercules, CA, USA), potassium iodide (KI), sodium azide (NaN3), sodium hydroxide (NaOH), copper sulfate pentahydrate (CuSO4•5H2O), diisopropyl ether, dichloromethane (CH2Cl2), ethyl acetate (EtOAc), tetrahydrofuran anhydrous (THF), hexane (HEX), methanol (MeOH), ethanol (EtOH) and acetone (CH3COCH3) were purchased from Sigma-Aldrich (St. Louis, MO, USA).
Sorroza-Martínez K., González-Méndez I., Vonlanthen M., Moineau-Chane Ching K.I., Caminade A.M., Illescas J, & Rivera E. (2020). First Class of Phosphorus Dendritic Compounds Containing β-Cyclodextrin Units in the Periphery Prepared by CuAAC. Molecules, 25(18), 4034.
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2

Synthesis of β-CD-PAMAM Conjugates

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All starting materials were commercially available reagent grade and were used without any further purification. β-Cyclodextrin (β-CD), PAMAM dendrimer G1 (PAMAM G1), propargyl bromide solution (80% by weight in toluene), p-toluenesulfonyl chloride (Cl-Ts), p-toluenesulfonic acid (OH-Ts), methyl 2-(4-hydroxyphenyl)acetate, N,N-dimethylformamide anhydrous (DMF), anhydrous potassium carbonate (K2CO3), dimethylsulfoxide (DMSO), ascorbic acid (H2Asc), N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (EDC·HCl), Bio-Gel P-10 medium from BIO-RAD, 1-hydroxybenzotriazole hydrochloride (HOBt·HCl), N,N-diisopropylethylamina (DIPEA), potassium iodide (KI), sodium azide (NaN3), sodium hydroxide (NaOH), copper sulfate pentahydrate (CuSO4·5H2O), dichloromethane (CH2Cl2), methanol (MeOH), ethanol (EtOH) and acetone (CH3COCH3) were purchased from Sigma-Aldrich.
Sorroza-Martínez K., González-Méndez I., Martínez-Serrano R.D., Solano J.D., Ruiu A., Illescas J., Zhu X.X, & Rivera E. (2020). Efficient modification of PAMAM G1 dendrimer surface with β-cyclodextrin units by CuAAC: impact on the water solubility and cytotoxicity. RSC Advances, 10(43), 25557-25566.
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3

Antioxidant Capacity Determination Protocol

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Potassium persulfate (99.5%), sodium carbonate (99%), Trolox (98%), 2,2-azinobis (3-ethylbenothiazoline-6-sulfonic acid) diammonium salt (ABTS) (98%), Folin Ciocalteu’s phenol reagent and Gallic acid (98%) were purchased from Sigma-Aldrich, South Africa. Iron (III) chloride 6-hydrate (97%), dimethyl sulfoxide (DMSO) (99.9%), Iron (II) sulfate 7-hydrate and acetic acid (87%); 2,4,6-Tri(2-pyridyl)-s-triazine (TPTZ) (99%), 2,2-diphenyl-1-picrylhydrazyl (DPPH) (96%), hydrochloric acid (35%), ascorbic acid (99%), sodium chloride (99.9%), and ethanol (99%) were purchased from BioRad, South Africa.
Aremu O.O., Oyedeji A.O., Oyedeji O.O., Nkeh-Chungag B.N, & Rusike C.R. (2019). In Vitro and In Vivo Antioxidant Properties of Taraxacum officinale in Nω-Nitro-l-Arginine Methyl Ester (L-NAME)-Induced Hypertensive Rats. Antioxidants, 8(8), 309.
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