All solvents were purified before use. N-bromosuccinimide, thiourea, 2-methylbenzyl chloride, 3-fluorobenzyl chloride, 2-chlorobenzyl chloride, 2,4-dichlorobenzyl chloride, 3,4-dichlorobenzyl chloride, 4-bromobenzyl chloride, 2-chloroacetamide, and ethyl chloroacetate were purchased from Acros Organics and used without purification. Compounds 2 , 3 , 4b , and 4h were prepared using methods described previously [10 ]. The reactions were monitored by thin-layer chromatography (TLC) using Fluka silica gel (60 F 254) plates (0.25 mm). Visualization was made with UV light. The melting points of the synthesized compounds were taken on a melting point tube. Infrared spectra were recorded on a Bruker Tensor 37 spectrometer (Germany). The 1H-NMR spectra were recorded on a Bruker WP 250 SY spectrometer (250.13 MHz) (Germany). Chemical shifts are reported relative to chloroform (δ=7.25 ppm) for 1H-NMR. The mass spectra were recorded on an Agilent LC/MSD SL 1100 instrument (USA).
2 chloroacetamide
Manufactured by Thermo Fisher Scientific
2-chloroacetamide is a chemical compound used in various laboratory applications. It functions as a reagent in organic synthesis and as a preservative in some biological samples. The core purpose of 2-chloroacetamide is to serve as a versatile tool in scientific research and analysis.
Automatically generated - may contain errors
Lab products found in correlation
Thiourea, by Thermo Fisher Scientific (1 mentions)
Lc msd sl 1100 instrument, by Agilent Technologies (1 mentions)
Tensor 37 spectrometer, by Bruker (1 mentions)
N bromosuccinimide, by Thermo Fisher Scientific (1 mentions)
Wp 250 sy spectrometer, by Bruker (1 mentions)
2 iodoacetamide, by Merck Group (1 mentions)
N n dimethylformamide (dmf), by Thermo Fisher Scientific (1 mentions)
Lead iodide, by Tokyo Chemical Industry (1 mentions)
Acetonitrile, by Merck Group (1 mentions)
Hydrochloric acid (hcl), by Merck Group (1 mentions)
2 propanol, by Merck Group (1 mentions)
Chlorobenzene, by Merck Group (1 mentions)
Cesium iodide, by Merck Group (1 mentions)
4 tert butylpyridine, by Merck Group (1 mentions)
Titanium isopropoxide, by Merck Group (1 mentions)
2 protocols using 2 chloroacetamide
1
Synthesis of Benzyl Substituted Heterocycles
2
Perovskite Solar Cell Fabrication
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The 2.5 × 2.5 cm2 fluorine-doped
tin oxide glass slides (FTO OPV-FTO22-15,
sheet resistance of 14 Ω·sq–1) were purchased
from OPVTech. Titanium isopropoxide (Ti[OCH(CH3)2]4, 97%), hydrochloric acid (HCl, 37%), 2-propanol (for
HPLC, 99.9%), chlorobenzene (CB, anhydrous 99.8%), acetonitrile (ACN,
99.8%), 4-tert-butylpyridine (TBP, 98.0%), and cesium
iodide (CsI, 99.999%) were purchased from Sigma Aldrich. Lead iodide
(PbI2, 99.99%) was purchased from Tokyo Chemical Industry
(TCI). PbBr2 (99.999%), methyl ammonium bromide (MABr,
>99.5%), and formamidinium iodide (FAI, >99.5%) were purchased
from
Lumtec. Bis(trifluoromethane)sulfonimide lithium salt (Li-TFSI, 99.0%), N,N-dimethylformamide (DMF, anhydrous >99.5%),
2-bromoacetamide (98%), and 2-chloroacetamide (98%) were purchased
from Acros. Dimethly sulfoxide (DMSO, >99.7%), 2-iodoacetamide
(98%),
and dimethyl sulfoxide-d6 (DMSO-d6) were purchased from Merck. Spiro-OMeTAD was
purchased from Borun New Material Technology. All chemical substances
obtained commercially were used as purchased without further purification.
tin oxide glass slides (FTO OPV-FTO22-15,
sheet resistance of 14 Ω·sq–1) were purchased
from OPVTech. Titanium isopropoxide (Ti[OCH(CH3)2]4, 97%), hydrochloric acid (HCl, 37%), 2-propanol (for
HPLC, 99.9%), chlorobenzene (CB, anhydrous 99.8%), acetonitrile (ACN,
99.8%), 4-tert-butylpyridine (TBP, 98.0%), and cesium
iodide (CsI, 99.999%) were purchased from Sigma Aldrich. Lead iodide
(PbI2, 99.99%) was purchased from Tokyo Chemical Industry
(TCI). PbBr2 (99.999%), methyl ammonium bromide (MABr,
>99.5%), and formamidinium iodide (FAI, >99.5%) were purchased
from
Lumtec. Bis(trifluoromethane)sulfonimide lithium salt (Li-TFSI, 99.0%), N,N-dimethylformamide (DMF, anhydrous >99.5%),
2-bromoacetamide (98%), and 2-chloroacetamide (98%) were purchased
from Acros. Dimethly sulfoxide (DMSO, >99.7%), 2-iodoacetamide
(98%),
and dimethyl sulfoxide-d6 (DMSO-d6) were purchased from Merck. Spiro-OMeTAD was
purchased from Borun New Material Technology. All chemical substances
obtained commercially were used as purchased without further purification.
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