Copper 1 iodide cui

Manufactured by Merck Group

Sourced in Germany

Copper(I) iodide (CuI) is a yellow, crystalline compound used in various laboratory applications. It functions as a reagent and a source of copper(I) ions. The compound's core function is to serve as a chemical building block and catalyst in various synthetic reactions and analytical procedures.

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4 protocols using copper 1 iodide cui

Brominated Pyrene Synthesis

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1,3,6,8-Tetrabromopyrene,
1-octyne, 1-dodecyne, bis(triphenylphosphine)palladium(II)
dichloride (Pd(PPh₃)₂Cl₂) and copper(I)
iodide (CuI) were procured from Sigma-Aldrich. The solvents, dichloromethane
(DCM) and petroleum benzine, were procured from Merck Ltd., and anhydrous
tetrahydrofuran (THF) and diisopropylamine were obtained from Sigma-Aldrich.

Bhagavathi Kandy S., Simon G.P., Cheng W., Zank J., Saito K, & Bhattacharyya A.R. (2019). Effect of Organic Modification on Multiwalled Carbon Nanotube Dispersions in Highly Concentrated Emulsions. ACS Omega, 4(4), 6647-6659.

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Synthesis of Cu(I) Coordination Polymer

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The reagents and solvents
were used without prior purification. Copper(I) iodide (CuI, 98%)
was purchased from Sigma-Aldrich (CAS: 7681–65–4), and
ligand 1,2-Bis(4-pyridyl)ethane (bpe, 98%) was purchased from Tokio
Company International (TCI) (CAS: 4916–57–8). The solvent
used both in the synthesis and in the preparation of the dispersions
is acetonitrile (CH₃CN), which was purchased from LabKem,
with HPLC degree of purification (CAS: 75–05–8). The
other two solvents used for the preparation of the dispersions are
methanol (MeOH) and dichloromethane (CH₂Cl₂)
obtained from Sigma-Aldrich and Thermo Scientific (CAS: 67–56–1,
75–09–2). The solvents used, isopropanol (C₃H₈O), N,N-dimethylformamide (DMF), and chloroform (CHCl₃), were purchased from Scharlau (CAS: 67–63–0,
68–12–2, 67–66–3); trichlorethylene (C₂HCl₃) was purchased from Sigma-Aldrich (CAS: 79–01–6);
acetone was purchased from Carlo Erba (CAS: 67–64–1);
and dimethyl sulfoxide (DMSO) was purchased from PanReac (CAS: 67–68–5).

García-Hernán A., Brito-Santos G., de la Rubia E., Aguilar-Galindo F., Castillo O., Lifante-Pedrola G., Sanchiz J., Guerrero-Lemus R, & Amo-Ochoa P. (2024). Determining Factors to Understand the External Quantum Efficiency Values: Study Carried Out with Copper(I)-I and 1,2-Bis(4-pyridyl)ethane Coordination Polymers as Downshifters in Photovoltaic Modules. Inorganic Chemistry, 63(10), 4646-4656.

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Synthesis of Colloidal Quantum Dots

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Copper(I) iodide (CuI, 99.999%, Sigma-Aldrich),
indium acetate In(Ac)₃, 99.99%, Alfa Aesar), 1-dodecanethiol
(DDT, 98%, Sigma-Aldrich), 1-octadecene (ODE, 90%, Acros), zinc stearate
(Zn(St)₂, Acros), mercaptopropionic acid (MPA, Sigma-Aldrich),
1-ethyl-3-(3-(dimethylamino)propyl)carbodiimide hydrochloride (EDC,
ThermoFisher), and NeutrAvidin (ThermoFisher). All solvents were purchased
from VWR International. Methanol, hexane, dimethylformamide, and ethyl
acetate were of pure grade. All of the water used in this study was
ultrapure 18MΩ·cm Millipore water obtained from a Direct-Q
3UV water filtration system.

Nguyen A.T., Baucom D.R., Wang Y, & Heyes C.D. (2023). Compact, Fast Blinking Cd-Free Quantum Dots for Super-Resolution Fluorescence Imaging. Chemical & Biomedical Imaging, 1(3), 251-259.

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Synthesis of Colloidal Quantum Dots

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Copper(I) iodide (CuI, 99.999%, Sigma-Aldrich),
indium acetate (InAc₃, 99.99%, Sigma-Aldrich), 1-dodecanethiol
(DDT, >98%, Sigma-Aldrich), ethanedithiol (EDT, >98%, Sigma-Aldrich),
indium-doped tin oxide substrates (ITO, ∼ 25 nm film thickness, R_sq ≤ 120 Ω/cm,^{2 (link)} PGO Germany), thin Indium-doped tin oxide substrates (ITO,
∼25 nm film thickness, total substrate thickness of ∼100
μm, R_sq ≤ 120 Ω/cm,^{2 (link)} PGO Germany), lithium perchlorate (LiClO₄, 99.99%, Sigma-Aldrich), and ferrocene (Fc, 98%, Sigma-Aldrich)
were used. Anhydrous solvents (methanol, 99.8%; butanol, 99.8%; and
toluene, 99.8%) and acetonitrile (99.99%) were all purchased from
Sigma-Aldrich. acetonitrile was dried before use in an Innovative
Technology PureSolv Micro column. All other chemicals were used as
received.

van der Stam W., de Graaf M., Gudjonsdottir S., Geuchies J.J., Dijkema J.J., Kirkwood N., Evers W.H., Longo A, & Houtepen A.J. (2018). Tuning and Probing the Distribution of Cu+ and Cu2+ Trap States Responsible for Broad-Band Photoluminescence in CuInS2 Nanocrystals. ACS Nano, 12(11), 11244-11253.

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