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Agilent 500 spectrometer

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The Agilent 500 spectrometer is a laboratory instrument used for spectroscopic analysis. It is designed to measure the absorption, emission, or scattering of electromagnetic radiation by samples. The core function of the Agilent 500 spectrometer is to provide accurate and reliable spectroscopic data to support analytical and research applications.

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Spectrometers (10 citations) Agilent 500 (8 citations) Agilent 500 MHz DD2 spectrometer (8 citations) Agilent 500 MHz NMR spectrometer (8 citations) Agilent DD2 500 MHz NMR spectrometer (4 citations) Agilent DD2 500 M NMR spectrometer (3 citations) 500 spectrometers (2 citations) Agilent DD2-500 spectrometer (2 citations)

7 protocols using agilent 500 spectrometer

1

NMR Spectroscopy of Aqueous Acetic Acid

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1H-NMR spectra were recorded in a deuterated aqueous solution of 2% acetic acid v/v. An Agilent 500 spectrometer was utilized (Agilent Technologies, Santa Clara, CA, USA) at room temperature. Spectra were internally referenced with tetramethylsilane (TMS) and calibrated using the residual solvent peaks.
Michailidou G., Zamboulis A, & Bikiaris D.N. (2023). Exploring the Blends’ Miscibility of a Novel Chitosan Derivative with Enhanced Antioxidant Properties; Prospects for 3D Printing Biomedical Applications. Marine Drugs, 21(7), 370.
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2

NMR Spectroscopy of Acetic Acid

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NMR spectra were recorded in a deuterated aqueous solution of acetic acid 2% v/v. An Agilent 500 spectrometer was utilized (Agilent Technologies, Santa Clara, CA, USA) at room temperature. Spectra were internally referenced with tetramethylsilane (TMS) and calibrated using the residual solvent peaks.
Ainali N.M., Xanthopoulou E., Michailidou G., Zamboulis A, & Bikiaris D.N. (2020). Microencapsulation of Fluticasone Propionate and Salmeterol Xinafoate in Modified Chitosan Microparticles for Release Optimization. Molecules, 25(17), 3888.
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3

NMR Characterization of Polyesters

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1H-NMR spectra of polyesters were obtained on an Agilent 500 spectrometer (Agilent Technologies, Santa Clara, CA, USA) at room temperature. Polymers were dissolved in deuterated trifluoroacetic acid (TFA-d) (5% w/v solutions). A total of 16 scans were recorded, and the sweep width was 6 kHz.
Papadopoulos L., Xanthopoulou E., Nikolaidis G.N., Zamboulis A., Achilias D.S., Papageorgiou G.Z, & Bikiaris D.N. (2020). Towards High Molecular Weight Furan-Based Polyesters: Solid State Polymerization Study of Bio-Based Poly(Propylene Furanoate) and Poly(Butylene Furanoate). Materials, 13(21), 4880.
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4

NMR Characterization of PEF Samples

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Nuclear magnetic resonance (NMR) spectra were recorded on an Agilent 500 spectrometer (Agilent Technologies, Santa Clara, CA, USA) and calibrated using the residual CDCl3 solvent peaks. PEF samples were dissolved in deuterated chloroform/deuterated trifluoroacetic acid mixtures. A dimethyl sulfoxide probe was also used for lock purposes for the 13C NMR spectra.
Stanley J., Terzopoulou Z., Klonos P.A., Zamboulis A., Xanthopoulou E., Koltsakidis S., Tzetzis D., Zemljič L.F., Lambropoulou D.A., Kyritsis A., Papageorgiou G.Z, & Bikiaris D.N. (2023). Effect of Monomer Type on the Synthesis and Properties of Poly(Ethylene Furanoate). Polymers, 15(12), 2707.
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5

NMR Spectroscopy of Organic Compounds

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NMR spectra were recorded in deuterated dimethylsulfoxide (DMSO-d6) or trifluoroacetic acid (TFA-d), on an Agilent 500 spectrometer (Agilent Technologies, Santa Clara, CA, USA), at room temperature. Spectra in TFA-d were recorded in the presence of a DMSO probe Spectra were internally referenced with tetramethylsilane (TMS) and calibrated using the residual solvent peaks.
Zamboulis A., Papadopoulos L., Terzopoulou Z., Bikiaris D.N., Patsiaoura D., Chrissafis K., Gazzano M., Lotti N, & Papageorgiou G.Z. (2019). Synthesis, Thermal Properties and Decomposition Mechanism of Poly(Ethylene Vanillate) Polyester. Polymers, 11(10), 1672.
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6

NMR Structural Characterization of Biocomposites

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NMR spectra were recorded in deuterated chloroform using an Agilent 500 spectrometer (Agilent Technologies, Santa Clara, CA, USA) for the structural study of the biocomposites at room temperature. Spectra were calibrated using the residual solvent peaks.
Papadopoulou K., Klonos P.A., Kyritsis A., Mašek O., Wurzer C., Tsachouridis K., Anastasiou A.D, & Bikiaris D.N. (2023). Synthesis and Study of Fully Biodegradable Composites Based on Poly(butylene succinate) and Biochar. Polymers, 15(4), 1049.
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7

Polyester Characterization by 1H-NMR

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1H-NMR spectra of polyesters (5% w/v) were recorded in deuterated chloroform (CDCl3), on an Agilent 500 spectrometer (Agilent Technologies, Santa Clara, CA, USA), at room temperature. The number of scans was 16 and the sweep width was 6 kHz.
Palamidi A., Kapourani A., Christodoulou E., Klonos P.A., Kontogiannopoulos K.N., Kyritsis A., Bikiaris D.N, & Barmpalexis P. (2021). Low Molecular Weight Oligomers of Poly(alkylene succinate) Polyesters as Plasticizers in Poly(vinyl alcohol) Based Pharmaceutical Applications. Polymers, 13(1), 146.
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