DSC measurements were conducted to characterize the solid-state of crystalline and amorphous samples. Samples (2 to 5 mg) were packed into standard aluminium crucibles (40 μL) with pierced lids. The samples were analysed with a DSC823e instrument (Mettler-Toledo, Greifensee, Switzerland) equipped with a cooling system (Julabo FT 900, Seelbach, Germany). Nitrogen (50 mL/min) was used as a purge gas. Equilibration at 25 °C for 3 minutes was followed by linear heating with a heating rate of 10 °C/min. Measurements were made in triplicate. Thermal events were analysed using the STARe software (Mettler-Toledo, Greifensee, Switzerland).
Dsc823e instrument
Manufactured by Mettler Toledo
Sourced in Switzerland
The DSC823e is a differential scanning calorimeter (DSC) instrument manufactured by Mettler Toledo. It is designed to measure the heat flow and temperature changes associated with physical and chemical transitions in materials as they are heated, cooled, or held at a constant temperature. The DSC823e provides quantitative and qualitative information about endothermic and exothermic processes, phase changes, and thermodynamic properties of a wide range of materials.
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Lab products found in correlation
2 protocols using dsc823e instrument
1
Solid-State Characterization by DSC
2
Reproducible DSC Thermogram Analysis
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DSC thermograms were recorded on a DSC823 e instrument (Mettler Toledo, Zurich, Switzerland) with an HSS7 sensor under a nitrogen atmosphere during a heating/cooling cycle (0→90→0 °C) with a heating and cooling rate of 3.5 °C/min. Each temperature cycle was sequentially repeated three times in order to ensure and check the reproducible response of the instrument. The sample concentration for DSC measurements was 2.0 wt. %.
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