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Autoflex 2 tof fof spectrometer

Manufactured by Bruker
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The Autoflex II ToF/FoF spectrometer is a high-performance analytical instrument designed for mass spectrometry applications. It utilizes time-of-flight (ToF) and Fourier transform ion cyclotron resonance (FT-ICR) technologies to provide accurate and sensitive detection of a wide range of molecular species. The core function of this instrument is to perform precise mass analysis and characterization of complex samples.

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Lab products found in correlation

Xevo qtof, by Waters Corporation (2 mentions) Trace gcms, by Thermo Fisher Scientific (2 mentions) Tqd mass spectrometer, by Waters Corporation (2 mentions) Vnmrs 600 spectrometer, by Agilent Technologies (2 mentions)

2 protocols using autoflex 2 tof fof spectrometer

1

Comprehensive Analytical Characterization

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NMR spectra were recorded in deuterated solvent solutions on a Varian VNMRS-600 spectrometer and referenced against solvent resonances ( 1 H, 13 C). ESMS data were recorded on a TQD mass spectrometer (Waters Ltd, UK) in either acetonitrile or methanol, GCMS data were recorded on a Trace GCMS (ThermoFinnigan) GCMS recorded in DCM, ASAP data were recorded on a Xevo QTOF (Waters) high resolution, accurate mass tandem mass spectrometer equipped with an Atmospheric Pressure Gas Chromatography (APGC) system and an Atmospheric Solids Analysis Probe (ASAP). MALDI data were recorded on a Bruker Autoflex II ToF/FoF spectrometer. Microanalyses were performed by the Elemental Analysis Service, London Metropolitan University, UK or Elemental Microanalysis Service, Durham University, UK. All chemicals were sourced from standard suppliers.
Davidson R., Hsu Y.T., Batchelor T., Yufit D, & Beeby A. (2016). The use of organolithium reagents for the synthesis of 4-aryl-2-phenylpyridines and their corresponding iridium(iii) complexes. Dalton transactions (Cambridge, England : 2003), 45(28).
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2

Analytical Characterization of Compounds

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General details. NMR spectra were recorded in deuterated solvent solutions on a Varian VNMRS-600 spectrometer and referenced against solvent resonances ( 1 H, 13 C).
ESMS data were recorded on a TQD mass spectrometer (Waters Ltd, UK) in either acetonitrile or methanol, GCMS data were recorded on Trace GCMS (ThermoFinnigan) GCMS recorded in DCM, ASAP data were recorded on a Xevo QTOF (Waters) high resolution, accurate mass tandem mass spectrometer equipped with Atmospheric Pressure Gas Chromatography (APGC) and Atmospheric Solids Analysis Probe (ASAP). MALDI data were recorded on a Bruker Autoflex II ToF/FoF spectrometer. Microanalyses were performed by Elemental Analysis Service, London Metropolitan University, UK or Elemental Microanalysis service, Durham University, UK.
Davidson R., Hsu Y.T., Griffiths G.C., Li C., Yufit D., Pal R, & Beeby A. (2018). Highly Linearized Twisted Iridium(III) Complexes. Inorganic chemistry, 57(22).
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