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Jeffamine d2000

Manufactured by Huntsman
Sourced in United States

Jeffamine D2000 is a polyetheramine product manufactured by Huntsman. It is a difunctional amine with a molecular weight of approximately 2,000 g/mol. Jeffamine D2000 serves as a building block in the formulation of various chemical products.

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2 protocols using jeffamine d2000

1

Polyetherdiamine Synthesis via Butyrolactone

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Example 13

A reaction vessel (round-bottom flask with stirrer, reflux condenser, water separator, and dropping funnel) was charged under a nitrogen atmosphere at 80° C. with 200.0 g (0.1 mol) of polyetherdiamine (Jeffamine D2000 from Huntsman). Over the course of 10 minutes, with stirring, 18.9 g (0.22 mol) of butyrolactone were added dropwise. The temperature was via 20-minute temperature ramps, by 10° C. in each case, to 200° C. maintained at this temperature for 6 hours. 0.4 g of p-toluenesulfonic acid was added and stirring continued at 250° C. for 6 hours more. Throughout the reaction time, the water of reaction was removed from the reaction mixture by distillation. The end product is a viscous liquid having an amine number of 6.5 mg KOH/g.

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2

Synthesis of Isocyanate-based Polyurethane Microcapsules

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The shell-forming isocyanate, a commercial methylene diphenyl diisocyanate (MDI) oligomer, Ongronat® 2500, and the monomeric IPDI, Desmodur® I, to be encapsulated, were kindly supplied by BorsodChem (Kazincbarcika, Hungary) and by Covestro AG (Leverkusen, Germany), respectively. The active (hydrogen) H source Jeffamine® D-2000, a polyetheramine, was supplied by Huntsman (The Woodlands, TX, USA). Regarding the emulsion stabilizers, the gum arabic (GA) was obtained from Fisher Chemical (Porto Salvo, Portugal), the Dabco® DC193 was purchased from Air Products, Dow Corning (Bristol, PA, USA), and the Polyvinyl alcohol (PVA), (98–99% hydrolyzed, of medium molecular weight (MW), with an average of 57,000 to 66,000 gmol−1) was obtained from Alfa Aesar (Haverhill, MA, USA). All the chemicals were used as received, without further purification.
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