Sta 449 f5 jupiter

Manufactured by Netzsch

Sourced in Germany

The STA 449 F5 Jupiter is a simultaneous thermal analysis (STA) instrument manufactured by Netzsch. It is designed to perform thermogravimetry (TG) and differential scanning calorimetry (DSC) measurements on a wide range of materials. The instrument provides accurate and reliable thermal analysis data to support various applications.

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Close spelling variants of this product

STA 449 F5/F3 Jupiter STA 449 F5 Jupiter instrument STA 449 F5 Jupiter Netzsch thermogravimeter STA 449 F5 STA 449

27 protocols using sta 449 f5 jupiter

Characterization of MIL-101(Fe) and MIL-GO Composites

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The morphologies of the synthesized MIL-101 (Fe), MIL-GO composite fillers and membranes were characterized by using Scanning Electron Microscope (SEM), LEO 1430 VP microscope (Leo Electron Microscopy Ltd, Cambridge, UK).
FTIR-ATR spectra of the synthesized MIL-101 (Fe), MIL-GO composite fillers and membranes were obtained by using Nicolet iS10 (Thermal Scientific, Waltham, USA) spectrometer in the range of 400–4000 cm⁻¹.
XRD analyses for the synthesized MIL-101 (Fe), and MIL-GO composite fillers were conducted by utilizing Philips X′′Pert (Malvern Panalytical, Malvern, UK). The transmission mode and 2θ range of 5–80° were applied.
The nitrogen adsorption/desorption measurements for the synthesized MIL-101 (Fe), and MIL-GO composite fillers were conducted at −195.7 °C via Gemini VI (Micromeritics Instrument Corp., Norcross, GA, USA). All samples were degassed for 6 h at 110 °C before the measurements.
Thermal properties of the synthesized MIL-101 (Fe), MIL-GO composite fillers and membranes were analyzed by using a Jupiter STA 449 F5 (Netzsch, Germany) thermogravimetric analyzer. TGA measurements were conducted from 25 °C to 950 °C under the nitrogen atmosphere.

Li G., Kujawski W., Knozowska K, & Kujawa J. (2022). Pebax® 2533/PVDF thin film mixed matrix membranes containing MIL-101 (Fe)/GO composite for CO2 capture. RSC Advances, 12(45), 29124-29136.

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Thermogravimetric Analysis of Samples

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The thermoanalyzer Jupiter STA 449 F5 (Netzsch, Germany) was used to conduct a thermogravimetric analysis of all samples. Samples were placed in aluminum oxide (Al₂O₃) crucible, then heated to 1050 °C, with a heating rate of 35 °C/min under a nitrogen atmosphere. The curves were examined using the Netzsch Proteus Analysis Software.

Al Hujran T.A., Magharbeh M.K., Habashneh A.Y., Al-Dmour R.S., Aboelela A, & Tawfeek H.M. (2022). Insight into the Inclusion Complexation of Fluconazole with Sulfonatocalix[4]naphthalene in Aqueous Solution, Solid-State, and Its Antimycotic Activity. Molecules, 27(14), 4425.

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Thermal Analysis of Pharmaceutical Mixtures

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The thermal properties of the physical, kneaded, and coevaporate mixture samples were evaluated using thermosanalyzer Jupiter STA 449 F5 (Netzsch, Germany). Thermogravimetric analysis (TGA), derivative thermogravimetry (DTG), were accomplished over a temperature range of 25–1100 °C. Sample were placed in the aluminum oxid crucible (Al₂O₃) and heated from 25 to 1100 °C with a heating rate of 20 °C/min under a nitrogen atmosphere. TGA and DTG were used for the thermal stability characterization of the investigated samples. The obtained curves were analyzed using the Netzsch Proteus Analysis Software.

Al Hujran T.A., Magharbeh M.K., Al-Gharabli S., Haddadin R.R., Al Soub M.N, & Tawfeek H.M. (2021). Studying the Complex Formation of Sulfonatocalix[4]naphthalene and Meloxicam towards Enhancing Its Solubility and Dissolution Performance. Pharmaceutics, 13(7), 994.

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Thermal Characterization of Solid Phase

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To identify the prepared solid phase, TG-DSC (analysis was performed using a Jupiter STA 449 F5 thermoanalyzer (Netzsch, Selb, Germany) with gaseous decomposition products identified in a Vertex 70v infrared spectrometer from Brüker Optik coupled to the thermoanalyzer. To perform this analysis, a stable sample was exposed to temperature. During this time, the thermoanalyzer time and temperature-dependent changes in the mass of the sample were recorded. The decomposition products were transported by capillary to the IR spectrometer, where they were analyzed in the infrared absorption spectra.

Cichosz M., Kiełkowska U., Skowron K., Kiedzik Ł., Łazarski S., Szkudlarek M., Kowalska B, & Żurawski D. (2022). Changes in Synthetic Soda Ash Production and Its Consequences for the Environment. Materials, 15(14), 4828.

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Thermogravimetric Analysis of Irradiated Samples

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The thermogravimetric analysis (TGA) of all samples (non-irradiated and UV-irradiated) was performed on the Jupiter STA 449 F5 thermoanalyzer by Netzsch coupled with the FT-IR Vertex 70V spectrometer by Bruker Optik in the following conditions: a nitrogen atmosphere, a temperature range of 20–600 °C, and a heating rate of 10°/min. The weight of the samples was 6–10 mg. The simultaneous measurement of TG, DTG, and DSC allowed for the determination of the following parameters: decomposition onset temperature (T₀), temperature (T_max) at the maximum process rate (V_max), weight loss (∆m) for individual stages, and heat effects (ΔH) accompanying the decomposition. The mixture of volatile products, released at temperatures ranging from room temperature to 600 °C, was analyzed based on the infrared spectra recorded in the range of 400–4000 cm⁻¹. The evolved gases were transported to the gas cell (with ZnSe spectrophotometric windows) in an FTIR spectrophotometer. The connections between the thermoanalyzer and spectrophotometer were heated to 200 °C to prevent condensation. The carrier gas shows no infrared absorption.

Bajer D, & Kaczmarek H. (2022). Thermal Stability of Fluorescent Chitosan Modified with Heterocyclic Aromatic Dyes. Materials, 15(10), 3667.

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Thermal Analysis of Material Properties

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Simultaneous thermogravimetric analysis (STA) was carried out on a NETZSCH STA 449 F5 Jupiter instrument (Berlin, Germany) using about 5–10 mg of the sample. The sample was placed in an alumina crucible and heated from 25 to 800 °C with a heating rate of 10 °C/min under nitrogen atmosphere, with a flow rate of 50 mL/min. In addition, differential scanning calorimetry (DSC) was carried out by using a Q200 V24.11 Build 124 TA instrument (New Castle, Delaware, USA). In a typical measurement, approximately 0.5 g of the sample was dispersed in DI water (the ratio 1:4 = sample: water) and stirred for 1 h. A small amount (5 mg) of dispersion was then placed in the pan and heated from 25 to 250 °C (a heating rate of 5 °C/min) under nitrogen atmosphere to observe the gelatinization temperature.

Watcharakitti J., Nimnuan J., Krusong K., Nanan S, & Smith S.M. (2023). Insight into the Molecular Weight of Hydrophobic Starch Laurate-Based Adhesives for Paper. Polymers, 15(7), 1754.

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Thermogravimetric Analysis of Precipitates

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Thermogravimetric analysis (TGA) of the precipitates obtained after 1 h of reaction time was carried out on an STA 449 F5 Jupiter thermal analyzer (Netzsch, Bayern, Germany) and Mettler TG 50 thermobalance (Mettler Toledo Corp., Zürich, Switzerland) equipped with a TC 10 TA processor. The measurements were performed in the stream of air and at a heating rate of 10 K min⁻¹.

Inkret S., Ćurlin M., Smokrović K., Kalčec N., Peranić N., Maltar-Strmečki N., Domazet Jurašin D, & Dutour Sikirić M. (2023). Can Differently Stabilized Silver Nanoparticles Modify Calcium Phosphate Precipitation?. Materials, 16(5), 1764.

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Thermal Analysis of R3 Samples

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For analyzing the reaction processes of the R³ samples, the samples were tested both by TGA and by a calorimeter.
For thermogravimetric analysis (TGA), “STA 449 F5 Jupiter” from NETZSCH (Selb, Germany) was employed. The crucibles consisted of alumina and were filled with 40–50 mg of powder material. To avoid oxidation, nitrogen was used as an inert gas. The samples were first heated up to 40 °C and kept constant at this temperature for 30 min. Subsequently, each sample was heated up to 1000 °C at a constant heating rate of 20 °C per minute.
For the calorimetric measurements, “MC CAL” from C3 Prozess- und Analysentechnik GmbH (Haar, Germany) was employed. For this, 20 g of R³ sample were prepared at room temperature and placed in the calorimeter ampoule, which was preconditioned at 40 °C. Measurements of the heat release of the R³ samples were carried out for seven days. The reference sample was used for the calculation of the specific heat capacity.

Weise K., Ukrainczyk N, & Koenders E. (2021). A Mass Balance Approach for Thermogravimetric Analysis in Pozzolanic Reactivity R3 Test and Effect of Drying Methods. Materials, 14(19), 5859.

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Thermal Analysis of Adhesive Samples

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A measure of 100 g of each prepared adhesive was poured into glass vials, and then freeze-dried to obtain solid uncured adhesives. These uncured adhesives were analyzed by thermogravimetric analysis (TGA) using a Netzsch STA 449 F5 Jupiter^® (Netzsch, Selb, Germany). The samples were scanned from room temperature to 400 °C at a rate of 10 °C/min under nitrogen.

Zhao Z., Sun S., Wu D., Zhang M., Huang C., Umemura K, & Yong Q. (2019). Synthesis and Characterization of Sucrose and Ammonium Dihydrogen Phosphate (SADP) Adhesive for Plywood. Polymers, 11(12), 1909.

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Thermal Analysis of Alumina Samples

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Thermal analyses were carried out using an STA 449 F5-Jupiter (Netzsch) device for TG and DTA measurements. The sample was placed in an Al₂O₃ crucible and heated up from 30°C to 800°C at a heating rate of 5°C min⁻¹ in a 20 ml min⁻¹ O₂ stream. An empty crucible was used as reference material. The TG curve was corrected using the data of a standard (Al₂O₃), which was measured with the same temperature program.

Gallo G., Terban M.W., Moudrakovski I., Huber T., Etter M., Ernst M., Hinrichsen B, & Dinnebier R.E. (2021). A previously unknown cyclic alkanolamine and molecular ranking using the pair distribution function. Acta Crystallographica Section B, Structural Science, Crystal Engineering and Materials, 77(Pt 6), 986-995.

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