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Dithiooxamide

Manufactured by Merck Group
Sourced in United States

Dithiooxamide is a chemical compound used as an analytical reagent in various laboratory applications. It serves as a chelating agent, forming colored complexes with certain metal ions. The core function of Dithiooxamide is to facilitate the detection and analysis of these metal ions in a variety of test samples.

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2 protocols using dithiooxamide

1

Determination of Heavy Metal Ions

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All reagents were analytical grade. Ultrapure water (18.2 MΩ·cm) from a Mill-Q system (Merck Millipore, Darmstadt, Germany) was used throughout. Laboratory containers were rinsed with H2O prior to use. Standard solutions of all metals (lead(II) nitrate, cadmium(II) nitrate tetrahydrate, potassium dichromate(VI), iron(III) chloride hexahydrate, nickel(II) sulfate hexahydrate, copper(II) sulfate pentahydrate, manganese(II) chloride tetrahydrate, magnesium(II) chloride hexahydrate, iron(II) sulfate heptahydrate, aluminum(III) sulfate hydrate, barium(II) chloride, vanadium(III) chloride, and cobalt(II) sulfate pentahydrate) were purchased from Sigma-Aldrich (St. Louis, MO, USA). L-ascorbic acid (97%), L-cysteine, Tris base (99.9%), bathophenanthroline (97%), dimethylglyoxime (99%), dithiooxamide (98.5%), and sodium fluoride were purchased from Sigma-Aldrich. Sodium acetate, ammonium acetate, hydrochloric acid, sodium hydroxide, and glacial acetic acid were obtained from Fisher Scientific (Pittsburgh, PA, USA). Whatman (grade 1) filter paper was purchased from Apollo Presentation Products (Booneville, MS, USA).
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2

Spectrophotometric Determination of Cr(III)

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All reagents used in this work were of analytical grade. Deionized water was used throughout the work. A 0.05-g amount of dithiooxamide (Sigma Aldrich, USA) was mixed in 20 mL of 1 mol L -1 NaOH, and diluted to 100 mL with water. The concentration of Cr(III) working solutions were prepared by dilution of 1 g L -1 Cr(III) solution (chromium(III) nitrate, Honeywell Fluka, German) with a 1 mmol L -1 of nitric acid.
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