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2 protocols using dimethylacetamide

1

Preparation of Functionalized Graphene Oxide

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Tryptone and yeast extract were purchased from Suzhou Biogene Biotechnology Co.,Ltd. Graphite powder, sulfuric acid (H2SO4), hydrochloric acid (HCl), hydrogen peroxide (H2O2), dimethylacetamide (DMAC), triethylamine (TEA), methacryloyl chloride (MAC), azobisisobutyronitrile (AIBN), methacrylic acid (MAA), butyl methacrylate (BMA), N-hydroxy succinimide (NHS), N,N’-Dicyclohexylcarbodiimide (DCC), 4-dimethylaminopyridine (DMAP), cyclohexanone, petroleum ether, ether and inorganic salts were all in analytical reagent grade were commercially obtained from Sinopharm Chemical Reagent Co.,Ltd. and used as received without further treatment. HPLC grade methanol was purchased from Shanghai Qiangshun Chemical Reagent Co.,Ltd. HPLC grade DMF was obtained from Tedia Company Inc.
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2

Bacterial Cellulose Hydrolysis and Analysis

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Bacterial cellulose was provided by Hainan Yida Co., Ltd. (Guangdong, China). Cellulase from Aspergillus niger (product #C0057, 10 000 U/g, slightly brown powder) was purchased from Okyo Chemical Industry (TCI). The following chemicals were purchased from Sinopharm Chemical Reagent Co., Ltd: dimethylacetamide (DMAc, ≥ 99%), lithium chloride (LiCl, ≥97%), sulfuric acid (≥98%), Avicel citric acid (≥99.5%), sodium citrate dihydrate (meets USP testing specifications), 3,5-dinitrosalicylic acid (DNS, ≥98%), ethyl alcohol (EtOH, ≥99%), acetone (≥
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