All commercial chemicals were used as supplied unless otherwise indicated. Microwave reactions were carried out in a Biotage Initiator+ w. Robot Eight Microwave System. Compounds were purified via flash chromatography using a Teledyne Combiflash RF-200 with RediSep columns (silica) and indicated mobile phase. All moisture sensitive reactions were performed under an inert atmosphere of ultra-pure argon with oven-dried glassware. 1H and 13C NMR spectra were recorded on a Varian 600 or Bruker 400 MHz spectrometers. Mass data were acquired using an Agilent 6230 TOF LC/MS spectrometer. Procedures for chemical synthesis, analytical characterization data, and original 1H and 13C NMR spectra for all tested compounds are described in Supporting Information .
Initiator w robot eight microwave system
Manufactured by Biotage
The Initiator+ w. Robot Eight Microwave System is a lab equipment product from Biotage. It is a microwave synthesis system designed for chemical reactions. The system includes a microwave reactor and a robotic arm for automated sample handling.
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Lab products found in correlation
2 protocols using initiator w robot eight microwave system
1
Microwave-assisted Organic Synthesis
2
Microwave-Assisted Organic Synthesis Protocol
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All commercial chemicals were used as supplied unless otherwise indicated. Microwave reactions were carried out in a Biotage Initiator+ w. Robot Eight Microwave System. Compounds were purified via flash chromatography using a Teledyne Combiflash RF‐200 with RediSep columns (silica) and indicated mobile phase. All moisture sensitive reactions were performed under an inert atmosphere of ultra‐pure argon with oven‐dried glassware. 1H and 13C NMR spectra were recorded on a Varian 600 or Bruker 400 MHz spectrometers. Mass data were acquired using an Agilent 6230 TOF LC/MS spectrometer. Procedures for chemical synthesis, analytical characterization data, and original 1H and 13C NMR spectra for all tested compounds are described in Supporting Information.
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