31P NMR analyses were performed at room temperature on a Bruker DPX 500 NMR spectrometer. The method described by Granata and Argyropoulos23 (link) was used. Cyclohexanol was used as an internal standard and chromium(
Dpx 500 nmr spectrometer
Manufactured by Bruker
The DPX 500 NMR spectrometer is a nuclear magnetic resonance (NMR) instrument produced by Bruker. It is designed to perform high-resolution NMR analysis on a variety of samples. The core function of the DPX 500 is to generate and detect radio frequency signals, which interact with the nuclear spins of the sample, allowing for the identification and quantification of chemical compounds.
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Lab products found in correlation
2 protocols using dpx 500 nmr spectrometer
1
Quantitative 31P NMR Analysis Protocol
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31P NMR analyses were performed at room temperature on a Bruker DPX 500 NMR spectrometer. The method described by Granata and Argyropoulos23 (link) was used. Cyclohexanol was used as an internal standard and chromium(iii) acetylacetonate as a relaxation agent. NMR tubes were provided with coaxial inserts filled with 85% H3PO4 and all chemical shifts were reported relative to the signal of phosphoric acid.
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31P NMR analyses were performed at room temperature on a Bruker DPX 500 NMR spectrometer. The method described by Granata and Argyropoulos23 (link) was used. Cyclohexanol was used as an internal standard and chromium(
2
Comprehensive NMR Characterization Protocol
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1H NMR spectra were obtained
in 5 mm NMR precision tubes at 298 K on either Bruker DPX-300 or DPX-400
NMR spectrometers. 1H NMR chemical shifts were internally
referenced to residual protiated solvent for DMSO-d6 (2.50 ppm), CD3OD (3.31 ppm), D2O (4.79 ppm), (CD3)2CO (2.05 ppm). 1H NMR spectra at variable temperature were obtained in 5 mm NMR precision
tube on a Bruker AV-III 400 NMR spectrometer. NOESY spectra were obtained
in 5 mm NMR precision tubes at 298 K on a Bruker DPX-500 NMR spectrometer. 1H NMR peaks were internally referenced to CHD2OD
(3.31 ppm) for methanol-d4 or 1,4-dioxane
(3.66 ppm). All data processing was carried out using MestReNova 9.0.1.
in 5 mm NMR precision tubes at 298 K on either Bruker DPX-300 or DPX-400
NMR spectrometers. 1H NMR chemical shifts were internally
referenced to residual protiated solvent for DMSO-d6 (2.50 ppm), CD3OD (3.31 ppm), D2O (4.79 ppm), (CD3)2CO (2.05 ppm). 1H NMR spectra at variable temperature were obtained in 5 mm NMR precision
tube on a Bruker AV-III 400 NMR spectrometer. NOESY spectra were obtained
in 5 mm NMR precision tubes at 298 K on a Bruker DPX-500 NMR spectrometer. 1H NMR peaks were internally referenced to CHD2OD
(3.31 ppm) for methanol-d4 or 1,4-dioxane
(3.66 ppm). All data processing was carried out using MestReNova 9.0.1.
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