The photobase generator (PBG) 2-(9-oxoxanthen-2-yl)propionic acid 1,5,7-triazabicyclo[4.4.0]dec-5-ene salt and 1,4-butanediol bis(thioglycolate) (dithiol, DT) were purchased from TCI Chemicals. Poly(ethylene glycol) diacrylate (PEGDA, Mn = 700 g mol−1), trimethylolpropane tris(3-mercoptopropianate) (trithiol, TT), triethylamine, 1-ethyl-3-methylimidazolium trifluoromethanesulfonate (EMIM Triflate), and sodium bicarbonate (NaHCO3) were purchased from Sigma–Aldrich. 4-Bromobenzenesulfonyl chloride was purchased from Alfa Aesar. Magnesium sulfate heptahydrate (MgSO4·7H2O) was obtained from Acros Organics. 1-Ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide (EMIM TFSI) was purchased from Solvionic. Finally, hydrochloric acid 37% (HCl) and dichloromethane (DCM) were obtained from VMR Chemicals.
2 9 oxoxanthen 2 yl propionic acid 1 5 7 triazabicyclo 4.4.0 dec 5 ene salt
Manufactured by Tokyo Chemical Industry
Sourced in Belgium
2-(9-oxoxanthen-2-yl)propionic acid 1,5,7-triazabicyclo[4.4.0]dec-5-ene salt is a chemical compound. It consists of 2-(9-oxoxanthen-2-yl)propionic acid combined with 1,5,7-triazabicyclo[4.4.0]dec-5-ene.
Automatically generated - may contain errors
Lab products found in correlation
1 ethyl 3 methylimidazolium trifluoromethanesulfonate emim triflate, by Merck Group (2 mentions)
Magnesium sulfate heptahydrate mgso4 7h2o, by Thermo Fisher Scientific (2 mentions)
Poly ethylene glycol diacrylate, by Merck Group (2 mentions)
1 4 butanediol bis thioglycolate dithiol dt, by Tokyo Chemical Industry (2 mentions)
Sodium bicarbonate nahco3, by Merck Group (1 mentions)
1 thioglycerol, by Merck Group (1 mentions)
Benzene 1 4 diboronicacid, by Apollo Scientific (1 mentions)
Triethylamine, by Merck Group (1 mentions)
2 protocols using 2 9 oxoxanthen 2 yl propionic acid 1 5 7 triazabicyclo 4.4.0 dec 5 ene salt
1
Photobase Generator Synthesis and Characterization
2
Photobase Generator Synthesis Protocol
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The photobase generator (PBG) 2-(9-Oxoxanthen-2-yl)propionic acid 1,5,7-triazabicyclo[4.4.0]dec-5-ene salt, 1,4-Butanediol Bis(thioglycolate) (dithiol, DT), and heptane were purchased from TCI Chemicals (Zwijndrecht, Belgium). Poly(ethylene glycol) diacrylate (PEGDA, Mn = 700 g·mol−1), trimethylolpropane tris(3-mercoptopropianate) (trithiol, TT), triethylamine, 1-Ethyl-3-methylimidazolium trifluoromethanesulfonate (EMIM Triflate), and 1-thioglycerol were purchased from Sigma-Aldrich (De Schnelldorf, Germany). Magnesium sulfate heptahydrate (MgSO4.7H2O) was obtained from Acros Organics (Geel, Belgium). Dichloromethane (DCM) was obtained from VMR Chemicals (Fontenay sous Bois, France). 1-Ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide (EMIM TFSI) was purchased from Solvionic (Toulouse, France). Finally, benzene-1,4-diboronic acid was purchased from Apollo Scientific (Stockport, UK).
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