Silver nitrate (AgNO3), chloroplatinic acid (H2PtCl6·6H2O), poly(vinylpyrrolidone) (PVP), anhydrous ethylene glycol (EG), and sodium chloride (NaCl) were purchased from Sigma Aldrich Chemical (Yongin, Kyeonggi-do, Korea) for the syntheses of AgNWs. A cycloaliphatic-type epoxy resin was purchased from Daicel Chemical Industry (Minato-ku, Tokyo, Japan). The anhydride-type curing agent, hexahydro-4-methylphthalic anhydride, and silver acetate (AgAc) were purchased from Sigma Aldrich Chemical. An imidazole-type catalyst, 1-(2-cyanoethyl)-2-ethyl-4-methylimidazole (imidazole), was purchased from TCI Chemical (Chuo-ku, Tokyo, Japan). The synthesized AgNW was purified using the washing method. Isopropyl alcohol (IPA), purchased from SK Chemical (Seongnam-si, Kyeonggi-do, Korea), was chosen as the solvent because of its low boiling point and capacity as a good stabilizer for AgNWs.
Hexahydro 4 methylphthalic anhydride
Manufactured by Merck Group
Sourced in United States
Hexahydro-4-methylphthalic anhydride is a chemical compound used in the production of various products. It serves as an important intermediate in various industrial processes. The compound has specific chemical properties that make it a useful component in certain applications.
Automatically generated - may contain errors
Lab products found in correlation
Anhydrous ethylene glycol, by Merck Group (1 mentions)
Silver acetate, by Merck Group (1 mentions)
Polyvinylpyrrolidone, by Merck Group (1 mentions)
Glutaric anhydride, by Merck Group (1 mentions)
Succinic anhydride, by Merck Group (1 mentions)
Diethylene glycol, by Merck Group (1 mentions)
1 5 7 triazabicyclo 4.4.0 dec 5 ene, by Merck Group (1 mentions)
Propylene glycol, by Merck Group (1 mentions)
Triphenylphosphine pph3, by Merck Group (1 mentions)
2 ethylhexanol, by Merck Group (1 mentions)
Ethylene glycol, by Merck Group (1 mentions)
Sodium hydroxide (naoh), by Avantor (1 mentions)
2 ethyl 4 methylimidazole, by Merck Group (1 mentions)
4 protocols using hexahydro 4 methylphthalic anhydride
1
Synthesis of Silver Nanowires
2
Synthesis of Epoxy Novolac Resin and Anhydrides
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Cardanol-derived
epoxy novolac resin NC547
was purchased from Cardolite (see Figure S1 in theSupporting Information for the chemical structure), whereas
hexahydro-4-methylphthalic anhydride (PAn), glutaric anhydride (GAn),
and succinic anhydride (SAn) were bought from Sigma-Aldrich. Triazabicyclodecene
(TBD), potassium (cubes in mineral oil, 99.5% trace metal basis),
and KPF6 (99.5% trace metal basis) were purchased from
Merck. Battery grade ethylene carbonate (EC) and diethyl carbonate
(DEC) were bought from Solvionic.
epoxy novolac resin NC547
was purchased from Cardolite (see Figure S1 in the
hexahydro-4-methylphthalic anhydride (PAn), glutaric anhydride (GAn),
and succinic anhydride (SAn) were bought from Sigma-Aldrich. Triazabicyclodecene
(TBD), potassium (cubes in mineral oil, 99.5% trace metal basis),
and KPF6 (99.5% trace metal basis) were purchased from
Merck. Battery grade ethylene carbonate (EC) and diethyl carbonate
(DEC) were bought from Solvionic.
3
Synthesis and Characterization of Epoxy Composites
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Bisphenol A diglycidyl ether (DGEBA) epoxy oligomer (Epon resin 828), accelerator composed of 2,4,6-tris-dimethylaminomethyl phenol (Epikure Curing Agent 3253) were kindly provided by Hexion Inc (Pueblo, CO, USA). Hexahydro-4-methylphthalic anhydride (HP), ethylene glycol (EG), diethylene glycol (DG), propylene glycol (PG), 2-ethyl-hexanol (2EH), ethylene glycol monobutyl ether (EGMBE) and 1,5,7-triazabicyclo[4,4,0]dec-5-ene (TBD), zinc acetylacetonate (Zn(Ac)2) and triphenylphosphine (PPh3) were purchased from Sigma-Aldrich (St. Louis, MO, USA) and used as received. Silicone mold releasing agent was purchased from Stoner (Quarryvile, PA, UAS). Sodium hydroxide (NaOH) was obtained from Avantor Performance Materials (Phillipsburg, NJ, USA).
4
Epoxy Resin Composite Synthesis
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Bisphenol A type epoxy resin, YD-128, was obtained from Kukdo Chemical (Seoul, Korea). Hexahydro-4-methylphthalic anhydride (HMPA), as the hardener for epoxy resin, and 2-ethyl-4-methylimidazole (EMI), as the catalyst, were purchased from Sigma-Aldrich (Yong-In, Korea). Furthermore, 2-(3,4-epoxycyclohexyl)ethyltrimethoxysilane (KBM-303), a coupling agent, was provided by Shln-Etsu Chemical Co., Ltd. (Tokyo, Japan). Aluminum oxides of spherical shapes with a median diameter of 14.4 μm (Al2O3, DAB-10SI) were purchased from Denki Kagaku Kogyo Kabushiki Kasisha (Tokyo, Japan). Boron nitride filler in the shape of a single-crystal platelet, with a mean particle size of ~45 μm and a surface area of 0.6 m2·g−1, was purchased from Momentive Performance Materials, Inc. (Waterford, NY, USA). All materials were directly used without purification or modification.
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