All manipulations were carried out under air. Distilled water was used directly from a Milli-Q purification system (Millipore, Burlington, MA, USA). Acetonitrile, ethanol, methanol (synthesis grade, Aldrich) were used as solvents as received. Tetraethyl orthosilicate (TEOS, 98% Aldrich, St. Louis, MI, USA), ammonium hydroxide solution (25%, Aldrich), 3-(Triethoxysilyl)propionitrile (97%, Aldrich), cis-cyclooctene (95%, Alfa Aesar, Karlsruhe, Germany), cyclooctene oxide (99%, Aldrich), cyclohexene (99%, Acros), cyclohexene oxide (98%, Aldrich), 2-cyclohexen-1-ol (95%, TCI, Tokyo, Japan) ), 2-cyclohexen-1-one (96%,TCI), cis-1,2-cyclohexanediol (99%, Acros, Geel, Belgium), cyclohexanol (99%, Alfa Aesar), cyclohexanone (99.8%, Acros) and TBHP (70% in water, Aldrich) were used as received.
Cis cyclooctene
Manufactured by Thermo Fisher Scientific
Sourced in Germany, United States
Cis-cyclooctene is a cyclic hydrocarbon compound with the molecular formula C8H14. It is a clear, colorless liquid that is used as a chemical intermediate in various industrial processes. The core function of cis-cyclooctene is to serve as a building block or precursor for the synthesis of other chemical compounds.
Automatically generated - may contain errors
Lab products found in correlation
Cyclohexene, by Thermo Fisher Scientific (2 mentions)
Cyclohexanol, by Thermo Fisher Scientific (2 mentions)
Cyclohexanone, by Thermo Fisher Scientific (2 mentions)
Milli q purification system, by Merck Group (2 mentions)
Cis 1 2 cyclohexanediol, by Thermo Fisher Scientific (2 mentions)
Acetonitrile, by Merck Group (2 mentions)
Ammonium hydroxide solution, by Merck Group (2 mentions)
Cyclooctene oxide, by Merck Group (2 mentions)
Cyclohexene oxide, by Merck Group (2 mentions)
Methanol, by Merck Group (1 mentions)
Ethanol, by Merck Group (1 mentions)
Tetraethyl orthosilicate teos, by Merck Group (1 mentions)
Tetraethyl orthosilicate, by Merck Group (1 mentions)
Diethyl ether, by Merck Group (1 mentions)
3 aminopropyltriethoxysilane, by Merck Group (1 mentions)
Limonene, by Merck Group (1 mentions)
Limonene oxide, by Merck Group (1 mentions)
Phosphotungstic acid hydrate, by Merck Group (1 mentions)
Acetophenone, by Merck Group (1 mentions)
Hydrogen peroxide, by Thermo Fisher Scientific (1 mentions)
3 protocols using cis cyclooctene
1
Synthesis and Characterization of Silica-Based Catalysts
2
Synthesis and Catalytic Evaluation of Cyclic Compounds
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All manipulations were carried out under air. Distilled water was used directly from a Milli-Q purification system (Millipore, Burlington, MA, USA). Acetonitrile, ethanol, methanol and diethyl ether (synthesis grade, Aldrich, St. Louis, MI, USA) were used as solvents and employed as received. Tetraethyl orthosilicate (TEOS, 98% Aldrich), ammonium hydroxide solution (25%, Aldrich), 3-aminopropyltriethoxysilane (APTES, 99%, Aldrich), cis-cyclooctene (CO, 95%, Alfa Aesar, Ward Hill, MA, USA), cyclooctene oxide (COE, 99%, Aldrich), cyclohexene (CH, 99%, Acros, Geel, Belgium), cyclohexene oxide (CHO, 98%, Aldrich), 2-cyclohexen-1-ol (CHol, 95%, TCI, Tokyo, Japan), 2-cyclohexen-1-one (CHone, 96%, TCI), cis-1,2-cyclohexanediol (CHD, 99%, Acros), limonene (Lim, 98%, Aldrich), limonene oxide (LO cis/trans mixture, 97%, Aldrich), (1S, 2S, 4R)-(+)-limonene-1,2-diol (ax-LD, 97%, Aldrich), L-carveol (Colcis/trans mixture, 95%, Aldrich), (R)-(-) Carvone (Cone 98%, Aldrich), cyclohexanol (CYol, 99%, Alfa Aesar, Karlsruhe, Germany), cyclohexanone (CYone, 99.8%, Acros), phosphotungstic acid hydrate (reagent grade, Aldrich), molybdatophosphoric acid hydrate (reagent grade, Merck, Darmstadt, Germany) and TBHP (70% in water, Aldrich) were used as received. The pure cis-LO, trans-LO and eq-LD were synthesized according to literature procedures [58 (link),59 (link),60 (link)].
3
Synthesis of Gold Nanoparticles on Silica
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Sources and purities of chemicals used were as follows: HAuCl4•3H2O (≥99.9% trace metals basis, Sigma-Aldrich), fumed silica (CAB-O-SIL90, Cabot Corporation), ethylenediamine (≥99% ReagentPlus, Sigma-Aldrich), ethanol (200 grade, Decon Labs), cobalt(II) nitrate hexahydrate (≥98%, Sigma-Aldrich), Nano H-ZSM-5 (P-26, ACS Material), decane (≥99% ReagentPlus, Sigma-Aldrich), dodecane (≥99% ReagentPlus, Sigma-Aldrich), cis-cyclooctene (95%, Alfa Aesar), EB (99.8% anhydrous, Sigma-Aldrich), EB-d10 (99 atomic % D, Sigma-Aldrich), 4-methylanisole (99%, Sigma-Aldrich), acetophenone (99% ReagentPlus, Sigma-Aldrich), 1-phenylethanol (98%, Sigma-Aldrich), hydrogen peroxide (30% aqueous solution, Fisher Chemical), potassium hydroxide (reagent grade, 90%, Sigma-Aldrich), sodium sulfate (Food Chemicals Codex/United States Pharmacopeia–grade, Fisher Chemical), tetrahydrofuran (>99%, Sigma-Aldrich), tert-butyl hydroperoxide (~5.5 M in decane, Sigma-Aldrich), PPh3 (>98.5%, Sigma-Aldrich), d -chloroform (99.8 atomic % D, Sigma-Aldrich), HCl (38% w/w, Fisher Chemical), HNO3 (68 to 70% w/w, Fisher Chemical), EM Quant peroxide test strips, and syringe filter (polyvinylidene difluoride membrane, 0.25 mm/0.2 μm, Acrodisc).
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