1 iododecane

Manufactured by Merck Group

Sourced in United States

1-iododecane is a chemical compound with the formula CH3(CH2)8CH2I. It is a straight-chain alkyl iodide that is commonly used as a reference standard and in organic synthesis reactions. The compound is a clear, colorless liquid at room temperature.

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Lab products found in correlation

1 iodobutane, by Merck Group (2 mentions) 1 iodopropane, by Merck Group (1 mentions) Naringenin, by Merck Group (1 mentions) Tetrahydrothiophene, by Merck Group (1 mentions) Sodium tetraphenylborate, by Merck Group (1 mentions) Labmaster 130, by MBraun (1 mentions) Lithium bis trifluoromethylsulfonyl imide, by J&K Scientific (1 mentions)

2 protocols using 1 iododecane

Synthesis of Naringenin Derivatives

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Reagents for chemical synthesis—naringenin, 1-iodopropane, 2-iodopropane, 1-iodobutane, and 1-iododecane—were purchased from Sigma-Aldrich Co. (St. Louis, MO, USA); hydroxylamine hydrochloride from LOBA Feinchemie GmbH (Fischamed, Austria); anhydrous sodium acetate, potassium carbonate and N,N-dimethylformamide (DMF) from Chempur (Piekary Śląskie, Poland). Anhydrous solvents for reactions (acetone and ethanol) were prepared according to standard procedures. All organic solvents were of analytical grade.

Kozłowska J., Grela E., Baczyńska D., Grabowiecka A, & Anioł M. (2019). Novel O-alkyl Derivatives of Naringenin and Their Oximes with Antimicrobial and Anticancer Activity. Molecules, 24(4), 679.

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Synthesis and Characterization of Ionic Liquids

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All synthetic experiments were carried out under nitrogen or argon using Schlenk techniques, since the iodide ILs are hygroscopic. Just the anion exchanges were carried out under air atmosphere. All products were stored in a glovebox (mBraun Labmaster 130) under argon atmosphere. 1‐iodobutane (99 %), 1‐iodoheptane (98 %), 1‐iododecane (98 %) and tetrahydrothiophene (99 %) were purchased from Sigma Aldrich, 1‐iodooctane (98 %) and 1‐iodohexane (98 %) from Acros Organics, 1‐iodopentane (98 %) from Alfa Aesar, 1‐iodononane (98 %) from TCI and sodium tetraphenylborate (99.5 %) from Merck. Lithium bis(trifluoromethylsulfonyl)imide was obtained from J&K. All chemicals were used without further purification. The sample of [(C₂H₅)₃S][NTf₂] was of commercial origin (Iolitech GmbH).

Schmitz A., Bülow M., Schmidt D., Zaitsau D.H., Junglas F., Knedel T., Verevkin S.P., Held C, & Janiak C. (2020). Tetrahydrothiophene‐Based Ionic Liquids: Synthesis and Thermodynamic Characterizations. ChemistryOpen, 10(2), 153-163.

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