Diacetone alcohol

Manufactured by Merck Group

Sourced in Germany

Diacetone alcohol is an organic compound with the chemical formula (CH3)2C(OH)CH2C(O)CH3. It is a colorless liquid with a distinct odor. The primary function of diacetone alcohol is as a solvent and intermediate in various chemical processes.

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4 protocols using diacetone alcohol

Zn-Zr Oxide Synthesis via Incipient Wetness

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Zn₁Zr₁₀O_z was synthesized with
Zn(NO₃)₂·6H₂O (Sigma-Aldrich,
reactant grade, 98%) and Zr(OH)₄ (MEL, XZO631/01) by the
incipient wetness impregnation method. The details of synthesis and
characterization could be found elsewhere.^{8 (link),24 (link)} Acetone
(J.T. Baker, 99.8%), H₂¹⁸O (Sigma-Aldrich, 97
atom % ¹⁸O), pyridine (J.T. Baker, 100%), diAcetone alcohol
(Sigma-Aldrich, 99%), and phorone_A (2,6-dimethyl-2,5-heptadien-4-one,
Oakwood Chemical, 99.93%) were used as purchased.

Li H., Guo D., Ulumuddin N., Jaegers N.R., Sun J., Peng B., McEwen J.S., Hu J, & Wang Y. (2021). Elucidating the Cooperative Roles of Water and Lewis Acid–Base Pairs in Cascade C–C Coupling and Self-Deoxygenation Reactions. JACS Au, 1(9), 1471-1487.

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ATV Characterization via Analytical Techniques

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The investigated sample of ATV was gifted from APL Research Centre Laboratories (a division of Aurobindo Pharma Ltd., Hyderabad.). Analytical reagent (AR grade) mesityl oxide, di acetone alcohol, o-xylene, methylene chloride, decane, ethanol, acetone, isopropyl alcohol (2-propanol), methyl tert-butyl ether, benzene, n-heptane, methyl isobutyl ketone (4-methyl-2-pentanone), toluene, and 1-methyl-2-pyrrolidinone were procured from Sigma-Aldrich (Steinheim, Germany). ACS grade formic acid was procured from Merck & HPLC water was procured from Merck, Mumbai, India.

Raju K.V., Pavan Kumar K.S., Siva Krishna N., Madhava Reddy P., Sreenivas N., Kumar Sharma H., Himabindu G, & Annapurna N. (2015). Trace Level Determination of Mesityl Oxide and Diacetone Alcohol in Atazanavir Sulfate Drug Substance by a Gas Chromatography Method. Scientia Pharmaceutica, 84(2), 321-331.

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Fabrication of Inkjet-Printed Ag/AgCl Electrodes

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A good method to fabricate fully inkjet printed Ag/AgCl reference electrodes has been described by Moya et al.^{92 (link)} NovaCentrix, Metalon (JS-B40G, Austin, TX) silver ink was used to print the silver layers on Kapton substrate and then sintered at 250 °C for 30 min. Then, PriElex Microchem (Westborough, MA) SU-8 ink was printed on top of the silver layers for passivation and then sintered 250 °C for 50 min. For chlorination, diluted NaClO (5 v/v% purchased from Sigma-Aldrich) was printed (2 passes) on the exposed silver and then washed with deionized water. For the formulation of a protecting membrane, a cocktail mixture of PVB (Butvar B-98) (10 w%) in methanol (40%), xylene (30%), diacetone alcohol (15%), and 1-butanol (15%), all purchased from Sigma-Aldrich, was printed (5 passes) on top of the chlorinated area. Lastly, the electrode was left in a fume hood to dry overnight.

Pandhi T., Cornwell C., Fujimoto K., Barnes P., Cox J., Xiong H., Davis P.H., Subbaraman H., Koehne J.E, & Estrada D. (2020). Fully inkjet-printed multilayered graphene-based flexible electrodes for repeatable electrochemical response. RSC Advances, 10(63), 38205-38219.

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Proteomics Sample Preparation Reagents

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Cytochrome c, myoglobin, ubiquitin, bovine serum albumin (BSA), hemoglobin, trypsin, mesityl oxide, diacetone alcohol, MS-grade trifluoroacetic acid (TFA), and formic acid were purchased from Sigma-Aldrich (Oakville, CA). Model peptides were purchased from GL Biochem Ltd. (Shanghai, China). HPLC-grade acetone, acetonitrile, and methanol were from Fisher Scientific (Ottawa, CA). Reagent-grade glacial acetic acid was from Caledon Laboratory Chemicals (Georgetown, CA), while reagent-grade ammonium hydroxide (28% solution) was from ACP Chemicals Inc. (Montreal, CA). Chemicals used for digestion, including urea, dithiothreitol (DTT), and iodoacetamide (IAA), were from Bio-Rad (Mississauga, CA). Throughout the study, Milli-Q purified water (18.2 MΩ cm) was used.

Güray M.Z., Zheng S, & Doucette A.A. (2017). Mass Spectrometry of Intact Proteins Reveals +98 u Chemical Artifacts Following Precipitation in Acetone. Journal of proteome research, 16(2).

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