Tg dsc sta 449 f3 jupiter

Manufactured by Netzsch

Sourced in Germany

The TG-DSC-STA 449 F3 Jupiter is a simultaneous thermal analysis (STA) instrument that combines thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) in a single measurement. It is used for the simultaneous analysis of weight changes and thermal effects in materials under controlled temperature and atmosphere conditions.

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Lab products found in correlation

Ir affinity 1 spectrometer, by Shimadzu (1 mentions) Ttrax 3 x ray diffractometer, by Rigaku (1 mentions) Supra 55, by Zeiss (1 mentions)

Spelling variants of this product

STA 449 F3 Jupiter (125 citations) STA 449 (21 citations) 449 F3 Jupiter (18 citations) TG/DSC (4 citations) TG-DSC STA-449 F3 (2 citations)

2 protocols using tg dsc sta 449 f3 jupiter

Synthesis and Characterization of IGZO Precursor Solution

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Indium(iii) nitrate hydrate (In(NO₃)₃·xH₂O, Sigma-Aldrich, 99.9%), gallium(iii) nitrate hydrate (Ga(NO₃)₃·xH₂O, Sigma-Aldrich, 99.9%) and zinc nitrate hexahydrate (Zn(NO₃)₂·6H2O, Sigma-Aldrich, 98%) were separately dissolved in 2-methoxyethanol (2-ME, C₃H₈O₂, Fisher Chemical, 99%) to produce metal precursor solutions with a concentration of 0.2 M. The fuel (urea, Sigma, 99%) was added to each solution and maintained under constant stirring for 1 h. In order to guarantee the redox stoichiometry of the reactions, the urea to indium nitrate, gallium nitrate and zinc nitrate molar proportions were (5/2):1, (5/2):1 and (5/3):1, respectively. IGZO precursor solution was prepared by combining the three precursor solutions made, to obtain an In₂O₃ : Ga₂O₃ : ZnO molar ratio of 1 : 3 : 1 with a 0.2 M concentration. The precursor solution was stirred for at least 36 h at room temperature and filtrated using a PTFE filter (0.45 μm) before use.
Thermogravimetry and differential scanning calorimetry (TG-DSC) (Netzsch, TG-DSC-STA 449 F3 Jupiter) were performed for the IGZO (1 : 3 : 1) solution under an air atmosphere up to 550 °C at a 10 °C min⁻¹ heating rate in an aluminum crucible.

Martins R.A., Carlos E., Deuermeier J., Pereira M.E., Martins R., Fortunato E, & Kiazadeh A. (2022). Emergent solution based IGZO memristor towards neuromorphic applications. Journal of Materials Chemistry. C, 10(6), 1991-1998.

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Solid-state NMR and Characterization of TBOSBL

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Solid-state ¹³C cross-polarization magic angle spinning
(CP-MAS) NMR spectra
of TBOSBL 1–3 were recorded on a
Bruker 400 spectrometer equipped with an 89 mm wide bore and a 9.4
T superconducting magnet with a spinning rate of 12 kHz and CP contact
time of 2 ms with a delay time of 2 s. FTIR spectra of TBOSBL
1–3 were collected using a Shimadzu IR
Affinity-1 spectrometer. P-XRD analysis data were collected using
a Rigaku TTRAX III X-ray diffractometer. TGA plots were recorded using
a TG-DSC STA 449 F3 Jupiter (NETZSCH, Selb, Germany) at a scan rate
of 10 °C/min under nitrogen flow (100 mL/min). FE-SEM images
were obtained using a Carl Zeiss AG instrument (model SUPRA 55). Porosity
and surface area were estimated using a Quantachrome Autosorb iQ₂ analyzer. In a typical gas experimental setup, TBOSBLs (80–120 mg) were charged in a 9 mm cell and were exposed
to degassing at 120 °C for 6–10 h by attaching to a degassing
unit. Subsequently, the cells with degassed polymeric samples were
filled up with helium gas and weighed accurately for analysis. Various
temperatures of the analysis unit sample cell were maintained using
a KGW isotherm bath (provided by Quantachrome), which was filled with
liquid N₂ (77 K), or a temperature-controlled bath (298
and 273 K).

Alam A., Mishra S., Hassan A., Bera R., Dutta S., Das Saha K, & Das N. (2020). Triptycene-Based and Schiff-Base-Linked Porous Networks: Efficient Gas Uptake, High CO2/N2 Selectivity, and Excellent Antiproliferative Activity. ACS Omega, 5(8), 4250-4260.

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