Trimethylene carbonate (TMC, Labso Chimie, France) was twice recrystallized from diethyl ether, δ-valerolactone (δ-VL, TCI Europe) was dried over CaH2 and freshly distilled prior to polymerization. Methoxy poly(ethylene oxide) (mPEO-OH, Mw = 5 kg mol−1, Đ = 1.12), benzyl alcohol (BnOH), and 1,5,7-triazabicyclo[4.4.0]dec-5-ene (TBD) were purchased from Sigma Aldrich. TBD was used as received. BnOH was dried with calcium oxide followed by vacuum distillation and stored over molecular sieves. mPEO-OH was dissolved in dichloromethane, precipitated in diethyl ether and dried under vacuum until constant weight. Dichloromethane (DCM, Penta, CZ) was dried over CaH2 and distilled prior to use. Sodium chloride (Lachema, CZ), sodium hydrogen carbonate (Lachema, CZ), potassium chloride (Lachema, CZ), di-potassium hydrogen phosphate trihydrate (Lachema, CZ), magnesium chloride (Lachema, CZ), calcium chloride (Lachema, CZ), sodium sulfate (Penta, CZ), tris-hydroxymethyl aminomethane (Sigma-Aldrich, Germany) and hydrochloric acid (Penta, CZ) were all used as received.
Benzyl alcohol bnoh
Manufactured by Merck Group
Benzyl alcohol (BnOH) is a colorless, viscous liquid commonly used as a solvent, preservative, and intermediate in various chemical processes. It has a mild, aromatic odor. Benzyl alcohol serves as a versatile laboratory reagent and can be utilized in a wide range of applications.
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Lab products found in correlation
Hydrochloric acid (hcl), by Merck Group (1 mentions)
Sodium sulfate, by Merck Group (1 mentions)
Tris hydroxymethyl aminomethane, by Merck Group (1 mentions)
1 5 7 triazabicyclo 4.4.0 dec 5 ene, by Merck Group (1 mentions)
Silver nitrate agno3, by Merck Group (1 mentions)
Hydrochloric acid (hcl), by Thermo Fisher Scientific (1 mentions)
Benzyl alcohol, by Merck Group (1 mentions)
1 2 dichlorobenzene dcb, by Merck Group (1 mentions)
Bismuth bromide bibr3, by Merck Group (1 mentions)
Acetonitrile mecn, by Merck Group (1 mentions)
Potassium iodide ki, by Merck Group (1 mentions)
2 protocols using benzyl alcohol bnoh
1
Synthesis and Purification of Polymers
2
Synthesis of Perovskite and Titanate Heterostructures
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Hombikat UV100 (UV100, Venator, Wynyard, UK), sodium hydroxide (NaOH, Fisher Scientific, Hampton, NH, USA), hydrochloric acid (HCl, 37%, Fisher Scientific) and deionized water (DI) were used to synthesize pristine hydrogen titanate. Bismuth bromide (BiBr3, Sigma-Aldrich, St. Louis, MO, USA), cesium bromide (CsBr, Sigma-Aldrich), dimethyl sulfoxide (DMSO, Sigma-Aldrich) and isopropanol (IPA, Sigma-Aldrich) was used to synthesize pristine Cs3Bi2Br9 and Cs3Bi2Br9/Hydrogen Titanate heterostructures. benzyl alcohol (BnOH, Sigma-Aldrich), Acetonitrile (MeCN, Sigma-Aldrich) and 1,2-dichlorobenzene (DCB, Sigma-Aldrich) were used for benzyl alcohol oxidation experiments. Potassium iodide (KI, Sigma-Aldrich), silver nitrate (AgNO3, Sigma-Aldrich), p-benzoquinone (p-BQ, Sigma-Aldrich) and tert-butyl alcohol (TBA, Sigma-Aldrich) were used for scavenger tests to identify the main reactive oxygen species (ROSs) responsible for BnOH conversion. All chemical reagents were used in purities >99% as received without any further purification.
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