X-ray diffraction measurements
were performed on a
TTRAX-III Rigaku diffractometer equipped with
a rotating Cu anode. The X-ray (Cu Kα radiation) tube voltages
and the current were 50 kV and 200 mA, respectively. The measurement
range of 2θ was from 10° to 120°, with a scan rate
of 2° per minute. Quantification of the phases and analysis of
the crystal structure parameters were performed using the JADE 2010
software. The open angles of the divergence and scattering slits were
both 0.51, and the width of the receiving slit was 0.15 mm.
Thomas B., Jardón-Álvarez D., Carmieli R., van Tol J, & Leskes M. (2023). The Effect of Disorder on Endogenous MAS-DNP: Study of Silicate Glasses and Crystals. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 127(9), 4759-4772.