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Chromafil pet 45 25

Manufactured by Macherey-Nagel
Sourced in Germany

Chromafil PET-45/25 is a syringe filter designed for sample preparation. It features a polyethylene terephthalate (PET) membrane with a pore size of 0.45 μm and an effective filtration area of 25 mm².

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3 protocols using chromafil pet 45 25

1

Textile Dye Extraction and Analysis

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The dye was extracted from both warp and weft textile samples (~0.002 g, fragments and original textile) using a solution of 5% Formic acid/MeOH at 100 °C for 10 min. Then, the solution was filtered (Chromafil PET-45/25, Macherey-Nagel, Düren, Germany) and a volume of 250 μL of the mixture MeOH; DMF (1:1, v/v) was added to the dry residue, then heated for 5 min at 100 °C. The extract obtained was used for UV-Vis i HPLC analysis.
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2

Explosive and Camouflage Material Preparation

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The standard stock solutions of explosives,
as well as military-purpose mixed explosives (Comp B and Octol), were
prepared in extra pure acetone (Sigma-Aldrich). The monomer solution
of carbazole was prepared in extra pure acetonitrile (AcCN). Gold
(III) chloride solution (HAuCl4 of 99.99% purity on trace
metals basis, containing ≤150.0 ppm trace metals, 30% by wt
in dilute HCl) was utilized for AuNP modification of the PBE memory-GC/PCz
working electrode surface, and the 0.04% (w/v) working solution was
prepared from this stock solution. The stock solutions of camouflage
materials (caffeine, paracetamol, aspartame, acetylsalicylic acid,
detergent, and d-glucose) at a concentration of 1000 mg L–1 were prepared in acetone and filtered through Chromafil
PET-45/25 (a 0.45 μm filter) (Macherey-Nagel) before measurements.
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3

Standardized Plant Material Preparation

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Dried and cut plant material was obtained from Alfred Galke GmbH (Bad Grund, Germany). Deuterated solvents for NMR spectroscopy were purchased from Euriso-top GmbH (Saarbrücken, Germany) and conventional 5 mm sample tubes were obtained from Rototec-Spintec GmbH (Griesheim, Germany). LC-MS grade formic acid, 1,2,4,5-tetrachloro-3-nitrobenzene (standard for quantitative NMR) were obtained from Sigma Aldrich Co. (St. Louis, MO, USA). Acetonitrile, methanol, water (all of LC-MS grade), and other (analytical grade) solvents were purchased from VWR International GmbH (Darmstadt, Germany). 0.45 and 0.20 µm pore size membrane filters (Chromafil PET-45/25 and PET-20/13) were obtained from Macherey-Nagel GmbH & Co. KG (Düren, Germany).
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