Potassium hexachloroiridate

Manufactured by Merck Group

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Potassium hexachloroiridate is a chemical compound with the formula K2[IrCl6]. It is a crystalline solid used as a standard reference material in various analytical techniques, such as atomic absorption spectroscopy and X-ray photoelectron spectroscopy, due to its well-defined chemical composition and stability.

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Potassium hexachloroiridate(IV)(K2IrCl6) (2 citations)

2 protocols using potassium hexachloroiridate

Bimetallic Catalyst Synthesis Protocol

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Tin chloride (SnCl₂; 98%, Sigma-Aldrich), Palladium chloride (PdCl₂; 99.8%, Sigma-Aldrich), nickel chloride hexahydrate (NiCl₂.6H₂O; 98%, Merck), tri-sodium citrate di-hydrate (Na₃C₆H₅O₇.2H₂O; 98%, Merck), ammonium chloride (NH₄Cl; 97%, Merck), sodium hypophosphite (NaH₂PO₂; 95%, Merck), aqueous ammonia solution (aq.NH₃; 27 wt%, Merck), nickel nitrate hexahydrate (Ni(NO₃)₂.6H₂O; 98%, Merck), iron nitrate nonahydrate (Fe(NO₃)₃; 98%, Merck), nickel sulfate hexahydrate (NiSO₄.6H₂O; 98%, Merck), ammonium molybdate ((NH₄)₆Mo₇O₂₄; 97%, Merck), sodium chloride (NaCl; 99%, Merck), Potassium Hydroxide pellets (KOH; 97%, Merck), hydrochloric acid (HCl; ~35%, Merck), sodium hydrogen citrate (Na₂C₆H₆O₇; 98%, Merck), potassium hexachloroiridate (K₂IrCl₆; 99%, Sigma-Aldrich), Pt/C (40 wt%, Sigma-Aldrich) and Ni-foam (Marketech International, USA) were used without further purification.

Sahasrabudhe A., Dixit H., Majee R, & Bhattacharyya S. (2018). Value added transformation of ubiquitous substrates into highly efficient and flexible electrodes for water splitting. Nature Communications, 9, 2014.

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Synthesis and Characterization of Electrode Materials

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Cu mesh (Alfa Aesar, 0.11 mm), cobalt(ii) sulphate heptahydrate (Co(SO₄)₂, 7H₂O; Merck, ≥98%), nickel(ii) sulphate heptahydrate (Ni(SO₄)₂, 7H₂O; Merck, ≥98%), potassium hydrogen carbonate (KHCO₃; Merck, ≥99.5%), ammonium per-sulphate solution (Lobachemie, ≥98%) ammonia solution (Merck, ≥25%), nickel(ii) chloride hexahydrate (NiCl₂·6H₂O; Merck, ≥99%), chromium(iii) chloride hexahydrate (CrCl₃·6H₂O; Merck, ≥96%), manganese(ii) chloride tetrahydrate (MnCl₂·4H₂O; Merck, ≥96%), sodium hydroxide (NaOH; Merck, ≥97%), sodium dodecyl sulphate (SDS; Merck, ≥98%), potassium hydroxide pellets (KOH; Merck, ≥85%), ethanol (C₂H₅OH; Merck ≥99.9%), Toray carbon fiber paper (CFP; Alfa Aesar), commercial Pt/C (40 wt%, Merck), ammonium molybdate ((NH₄)₆Mo₇O₂₄; 97%, Merck), sodium chloride (NaCl; 99%, Merck), sodium hydrogen citrate (Na₂C₆H₆O₇; 98%, Merck), potassium hexachloroiridate (K₂IrCl₆; 99%, Sigma-Aldrich), nickel nitrate hexahydrate (Ni(NO₃)₂·6H₂O; 98%, Merck), iron nitrate nonahydrate (Fe(NO₃)₃·9H₂O; 98%, Merck) and Nafion perfluorinated resin solution (5 wt%, Merck) were used without further purification.

Parvin S., Kumar A., Ghosh A, & Bhattacharyya S. (2020). An earth-abundant bimetallic catalyst coated metallic nanowire grown electrode with platinum-like pH-universal hydrogen evolution activity at high current density. Chemical Science, 11(15), 3893-3902.

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