The following were purchased from Sigma-Aldrich: 4-phenylazophenol (98%), 1-chlorohexane (99%), 1-chlorodecane (98%), dibutyltin dilaurate (DBTDL, 95%), and butyl acrylate (>99%). Potassium carbonate (>99%), potassium iodide (>99.5%), 6-chloro-1-hexanol (>96%), 1-chlorotetradecane (>98%), and 1-chlorooctadecane (>98%) were purchased from Tokyo Chemical Industry Co., Ltd. The following were purchased from Samchun Chemicals Co., Ltd.: 2,2′-azobisisobutyronitrile (98%), 2-butanone (MEK, 99.5%), N,N-dimethylformamide (DMF, 99.5%), tetrahydrofuran (THF, 99.9%), methanol (99.5%), n-hexane (96%), acetone (99.5%), and ethyl acetate (EA, 99.5%). Lastly, 2-isocyanatoethyl acrylate (Karenz AOI, Showa Denko) was used as the isocyanate-containing acrylic monomer.
1 chlorodecane
Manufactured by Merck Group
1-chlorodecane is a straight-chain alkyl halide with a carbon chain length of 10 and a chlorine atom attached at the first carbon position. It is a colorless, oily liquid commonly used as a chemical intermediate and solvent in various industrial applications.
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Lab products found in correlation
2 protocols using 1 chlorodecane
1
Synthesis of Functionalized Polymers
2
Quantification of Disinfection By-Products
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Standards of THMs (bromoform, chloroform, bromodichloromethane, dibromochloromethane) and other neutral DBPs, viz. HANs (dichloroacetonitrile, dibromoacetonitrile, bromochloroacetonitrile, trichloroacetonitrile), HKs (1,1-dichloro-2-propanone and 1,1,1-trichloro-2-propanone) and a HNM (trichloronitromethane), and HAAs (monochloroacetic acid, monobromoacetic acid, dichloroacetic acid, dibromoacetic acid, trichloroacetic acid, bromochloroacetic acid, bromodichloroacetic acid, chlorodibromoacetic acid and tribromoacetic acid) were from Restek, acquired from Teknolab Sorbent (Kungsbacka, Sweden). Additional standards of 1,2-dibromopropane (97%) and 1-chlorodecane were acquired from Sigma-Aldrich (Stockholm, Sweden).
Stock solutions in methanol containing 0.2 μg μL−1 (stock solution 1, TableS1 ), 0.02 μg μL−1 (stock solution 2), and 0.002 μg μL−1 (stock solution 3) were prepared for every THM, HAN, HK, HNM, and HAA (see Table S1 in supplementary information for details). The stock solutions were added to samples of Milli-Q water for calibration, as well as to MtBE for direct GC-XSD determination. The surrogate standard 1,2-dibromopropane was prepared in methanol and the recovery standard 1-chlorodecane was prepared in MTBE.
Stock solutions in methanol containing 0.2 μg μL−1 (stock solution 1, Table
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