Silica gel 60 preparative thin layer chromatographic plates

Manufactured by Merck Group

Silica gel 60 preparative thin-layer chromatographic plates are a type of laboratory equipment used for the separation and purification of chemical compounds. They consist of a thin layer of silica gel, which is an adsorbent material, coated onto a rigid support such as glass or aluminum. These plates are designed for preparative-scale thin-layer chromatography, a technique that allows for the separation and isolation of compounds from complex mixtures.

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Silica gel 60, by Merck Group (2 mentions)

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3 protocols using silica gel 60 preparative thin layer chromatographic plates

Flash Chromatography Purification of Compounds

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All reagents were purchased from Sigma-Aldrich
and used as received, except for pyrrole, which was distilled and
stored in the freezer. Silica gel 60 (0.04–0.063 mm particle
size, 230–400 mesh, Merck) was employed for flash chromatography.
Silica gel 60 preparative thin-layer chromatographic plates (20 cm
× 20 cm × 0.5 mm, Merck) were used for final purification
of all compounds.

Larsen S., Adewuyi J.A., Ung G, & Ghosh A. (2023). Transition-Metal Isocorroles as Singlet Oxygen Sensitizers. Inorganic Chemistry, 62(19), 7483-7490.

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Synthesis of Free-base Corroles

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Free-base
corroles were synthesized via the
so-called water–methanol method.^{20 (link)} All other reagents were purchased from Sigma-Aldrich (Merck) and
used as received. Silica gel 60 (0.04–0.063 mm particle size,
230–400 mesh, Merck) was employed for flash chromatography.
Silica gel 60 preparative thin-layer chromatographic plates (20 cm
× 20 cm × 0.5 mm, Merck) were used for final purification
of all complexes.

Alemayehu A.B., McCormick-McPherson L.J., Conradie J, & Ghosh A. (2021). Rhenium Corrole Dimers: Electrochemical Insights into the Nature of the Metal–Metal Quadruple Bond. Inorganic Chemistry, 60(11), 8315-8321.

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Synthesis of Free-Base Corroles

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Unless otherwise mentioned, all chemicals were obtained from Merck. Silica gel 60 (0.04-0.063 mm particle size, 230-400 mesh) was employed for flash chromatography. Silica gel 60 preparative thin-layer chromatographic plates (20 cm ×20 cm, 0.5 mm thick, Merck) and aluminum oxide 60 preparative thin-layer chromatographic plates (20 cm × 20 cm, 1.5 mm thick, Merck) were used for final purification of all complexes. Free-base corroles were prepared according to previously reported procedures^{22 ,23 (link)}.

Thomassen I.K., McCormick-McPherson L.J., Borisov S.M, & Ghosh A. (2020). Iridium Corroles Exhibit Weak Near-Infrared Phosphorescence but Efficiently Sensitize Singlet Oxygen Formation. Scientific Reports, 10, 7551.

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