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2 2 azobis isobutyronitrile

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Sourced in China

2,2-azobis(isobutyronitrile) is a chemical compound commonly used as an initiator in free-radical polymerization reactions. It is a white crystalline solid with the chemical formula C8H12N4. The compound decomposes at high temperatures, generating nitrogen gas and free radicals that can initiate the polymerization of various monomers.

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Lab products found in correlation

Ethylene glycol dimethacrylate, by Adamas (2 mentions) Dimethylaminoethyl methacrylate, by Adamas (2 mentions) 1 1 bi 2 naphthol, by Adamas (2 mentions) Milli q gradient system, by Merck Group (1 mentions) 3 aminopropyltriethoxysilane aptes, by Thermo Fisher Scientific (1 mentions) Gossypol, by Merck Group (1 mentions) Quercetin, by Adamas (1 mentions) Acrylamide, by Adamas (1 mentions) Sodium hydroxide (naoh), by Sinopharm (1 mentions) Trimethylamine, by Sinopharm (1 mentions) N methyl imidazole, by Sinopharm (1 mentions) 1 methyl 2 pyrrolidone, by Sinopharm (1 mentions) Poly 2 6 dimethyl 1 4 phenylene oxide ppo, by Merck Group (1 mentions) Silver nitrate, by Sinopharm (1 mentions) Sodium sulfate, by Sinopharm (1 mentions)

3 protocols using 2 2 azobis isobutyronitrile

1

Synthesis and Characterization of Molecularly Imprinted Polymers

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Gossypol was purchased from Sigma-Aldrich (Shanghai, China). Dimethylaminoethyl methacrylate (DMAEMA), ethylene glycol dimethacrylate (EGDMA), divinylbenzene (DVB), 1,1’-bi-2-naphthol, and 2,2-azobis(isobutyronitrile) (AIBN) were purchased from Adamas Reagent Co., Ltd. (Shanghai, China). Hexaphenol was purchased from WAKO Pure Chemical Industry, Ltd. (in Japan). Tetraethoxysilane (TEOS), ellagic acid, and quercetin were obtained from Adamas (Shanghai, China). Silica beads (0.5 μm average particle size) and (3-aminopropyl) triethoxysilane (APTES) were purchased from Alfa Aesar (Shanghai, China). Methanol, acetone, hydrochloric acid, acetic acid, and sodium hydroxide were all analytical grade and purchased from Tianjin Zhiyuan Chemical Co., Ltd. (Tianjin, China). Water was purified by a Millipore Milli-Q gradient system (Massachusetts, America) to HPLC grade.
Wang L., Zhi K., Zhang Y., Liu Y., Zhang L., Yasin A, & Lin Q. (2019). Molecularly Imprinted Polymers for Gossypol via Sol–Gel, Bulk, and Surface Layer Imprinting—A Comparative Study. Polymers, 11(4), 602.
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2

Synthesis of Organic Compounds

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All reagents and deuterated solvents were obtained commercially unless otherwise noted (All reagents were used as received). Starting material and Hoveyda–Grubbs catalyst 2nd generation were purchased from Alfa-Aesar, Aldrich, Acros, Adamas and Ark pharm Reagent Co., Ltd. (Shanghai, China). Butylated hydroxyanisole (BHA), 2,6-di-tert-butyl-4-methylphenol (BHT), dimethylaminoethyl methacrylate (DMAEMA), acrylamide (AM), ethylene glycol dimethacrylate (EGDMA), 1,1′-bi-2-naphthol and 2,2-azobis(isobutyronitrile) (AIBN) were purchased from Adamas Reagent Co., Ltd. (Shanghai, China).
Wang L., Lin Q., Zhang Y., Liu Y., Yasin A, & Zhang L. (2019). Design and synthesis of supramolecular functional monomers bearing urea and norbornene motifs. RSC Advances, 9(35), 20058-20064.
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3

Bromination of Poly(2,6-dimethyl-1,4-phenylene oxide)

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Poly(2,6-dimethyl-1,4-phenylene
oxide) (PPO) was purchased from Sigma-Aldrich Co., Ltd., P. R. China.
2,2′-Azobisisobutyronitrile (AIBN) and N-bromosuccinimide
(NBS) were purchased from Adamas Reagent Co., Ltd., China. Chlorobenzene
was bought from Shanghai Titas Co., Ltd., P. R. China. Potassium chromate
(K2CrO4), trimethylamine, N-methylimidazole, sodium sulfate (Na2SO4), N-methypyrrolidine, sodium hydroxide (NaOH), N-methylpiperidine, chloroform (CHCl3), sodium chloride
(NaCl), silver nitrate (AgNO3), ethanol (EtOH), and 1-methyl-2-pyrrolidone
(NMP) were obtained from Sinopharm Chemical Reagent Co., Ltd., P.
R. China and were utilized as attained. Deionized (DI) water was utilized
throughout the work.
Khan M.I., Li X., Fernandez-Garcia J., Lashari M.H., ur Rehman A., Elboughdiri N., Kolsi L, & Ghernaout D. (2021). Effect of Different Quaternary Ammonium Groups on the Hydroxide Conductivity and Stability of Anion Exchange Membranes. ACS Omega, 6(12), 7994-8001.
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