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2 protocols using cis 3 hexenyl hexanoate

1

Characterization of Volatile Compounds

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β-Myrcene (≥90.0%) and cis-3-Hexenyl hexanoate (98%) were purchased from Macklin Biochemical Co. Ltd. (Shanghai, China). Benzylalcohol (≥99.5%), Linalool (98%), Nonanal (96%), α-Terpineol (>95.0%), Geraniol (≥99.0%), cis-Jasmone (98%), α-Farnesene (98%), and methyl palmitate (99%) were obtained from Aladdin Biochemical Co. Ltd. (Shanghai, China). Linalool oxide (pyranoid) and trans-Nerolidol were purchased from Yuanye Bio-Technology Co. Ltd. (Shanghai, China). n-Alkane mixtures of C7–C40 were supplied by Sigma-Aldrich Trading Co. Ltd. (Shanghai, China) and used to determine retention indices (RI). Ethyl decanoate was used as the internal standard and purchased from Aladdin Biochemical Co. Ltd. (Shanghai, China). Ultra-pure water was obtained using a Milli-Q purification system (Millipore, Bedford, MA, USA). Distilled water was purchased from the Hangzhou Wahaha Group Co. Ltd. (Hangzhou, China).
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2

Comprehensive Chemical Sourcing for Analytical Experiments

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Anhydrous
sodium sulfate (AR grade) was purchased from GHTECH (Shantou, Guangdong,
China); dichloromethane (AR grade) was ordered from PN-CHEM (Zhengzhou,
Henan, China). Tridecanol, 2-hexenal, 2-heptanol, (Z)-3-hexenyl acetate,
decanal, and benzyl nitrile were purchased from Sigma (St. Louis,
Missouri, USA); α-farnesene, cis-3-hexenyl hexanoate, 1-hexanol,
(Z)-3-hexenol, benzaldehyde, phytol acetate, ethyl decanoate, 3-octanol,
and guaiacol were obtained from Macklin (Shanghai, China); β-ocimene,
α-copaene, germacrene D, and neophytadiene were purchased from
J&K Chemicals (Shanghai, China); cis-jasmone, caffeine, and (E)-2-hexenol
were obtained from ChemFaces (Wuhan, China); indole was purchased
from Solarbio (Beijing, China); benzyl alcohol, linalool, geraniol,
nerol, nerolidol, α-terpinene, α-humulene, hexadecanoic
acid methyl ester, phytol, phenylacetaldehyde, α-terpineol,
2-phenylethanol, 1-octen-3-ol, δ-cadinene, caryophyllene oxide,
neral, methyl salicylate, and linalool oxide were purchased from Yuanye
Bio-Technology Co. (Shanghai, China). The alkane standard (C6–C44) was purchased from AccuStandard (New Haven,
CT, USA).
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