Carboxylic acid and amine difunctionalized PEGs (∼250 g mol−1), 4-pyridinecarboxaldehyde, 4-pyridinemethanol, and tris(bipyridine)ruthenium(ii ) chloride were purchased from Sigma-Aldrich. Ethyl formate, phosphorus(v ) oxychloride, tert-butylamine, ascorbic acid, and the other reagents were of analytical grade and used without further purification. Isocyanide tert-butane was synthesized according to the literature.32 (link)
Tris bipyridine ruthenium ii chloride
Manufactured by Merck Group
Sourced in Australia
Tris(bipyridine)ruthenium(ii) chloride is a coordination compound with the chemical formula C30H24Cl2N6Ru. It is a light-sensitive, orange-red crystalline solid that exhibits luminescent properties. The compound is widely used as a reagent in various applications, particularly in the field of analytical chemistry and photochemistry.
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2 protocols using tris bipyridine ruthenium ii chloride
1
Synthesis of Ruthenium-Based Photocatalysts
2
Electrochemical Sensing with Plasmonic Probe
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Phosphate buffer solution (PBS, 0.1 mol L -1 , pH = 7.4) containing 1.0 mmol L -1 tris(bipyridine) ruthenium(II) chloride (99.95%, Sigma-Aldrich, Australia) and a varied concentration of tripropylamine (TPrA 98%, Sigma-Aldrich, ranging from 0-20 mmol L -1 )
was injected from the inlet (see Figure 2). The flow was subsequently passed through the channel over the reference electrode (RE, AgCl/Ag wire), followed by the fiber optic plasmonic probe (i.e. working electrode), and finally the counter electrode (CE, coiled platinum wire). Fluid motion was maintained at a flow rate of 0.050 mL min -1 by a programmable PHD 2000 syringe pump (Harvard Apparatus, USA). The flow injection device was first tested with water to ensure that a reproducible and previously reported transmission spectrum [43] was observed. All measurements were conducted at 25 o C.
was injected from the inlet (see Figure 2). The flow was subsequently passed through the channel over the reference electrode (RE, AgCl/Ag wire), followed by the fiber optic plasmonic probe (i.e. working electrode), and finally the counter electrode (CE, coiled platinum wire). Fluid motion was maintained at a flow rate of 0.050 mL min -1 by a programmable PHD 2000 syringe pump (Harvard Apparatus, USA). The flow injection device was first tested with water to ensure that a reproducible and previously reported transmission spectrum [43] was observed. All measurements were conducted at 25 o C.
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