Ecz600 spectrometers

Manufactured by JEOL

The ECZ600 spectrometers are advanced electron spin resonance (ESR) systems manufactured by JEOL. They are designed to perform high-precision analysis of paramagnetic materials and radical species. The ECZ600 spectrometers offer a wide magnetic field range and superior signal-to-noise ratio, enabling researchers to obtain accurate and reliable data in their investigations.

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Lab products found in correlation

Silica gel 60n, by Kanto Chemical (1 mentions) Cosmosil 5c18 ar 2, by Nacalai Tesque (1 mentions) Pack sil 06, by YMC (1 mentions) Diaion hp 20, by Mitsubishi (1 mentions) Sephadex lh 20, by GE Healthcare (1 mentions) Uv mini 1240 spectrometer, by Shimadzu (1 mentions) Ft ir 230 spectrophotometer, by Jasco (1 mentions) Lcms 2020 spectrometer, by Shimadzu (1 mentions)

2 protocols using ecz600 spectrometers

Purification of Natural Products

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NMR spectra were recorded on JEOL ECZ600 spectrometers in a deuterated solvent whose chemical shift was used as an internal standard. Column chromatography was performed using Silica Gel 60N (Kanto Chemical Co., Tokyo, Japan), Chromatorex ODS (Fuji Silysia Chemical Ltd., Kasugai, Japan), Diaion HP-20 (Mitsubishi Chemical Co., Tokyo, Japan) and Sephadex LH-20 (GE Healthcare Japan, Tokyo, Japan). Preparative HPLC was performed using YMC-Pack SIL-06 (YMC Co. Ltd., Kyoto, Japan), COSMOSIL 5C₁₈-AR-II, COSMOSIL Cholester, COSMOSIL πNAP (Nacalai Tesque, Inc. Kyoto, Japan) and CAPCELL PAK C₁₈ MGII (OSAKA SODA Ltd., Osaka, Japan).

Arai M.A., Morita K., Kawano H., Makita Y., Hashimoto M., Suganami A., Tamura Y., Sadhu S.K., Ahmed F, & Ishibashi M. (2020). Target protein-oriented isolation of Hes1 dimer inhibitors using protein based methods. Scientific Reports, 10, 1381.

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Comprehensive Spectroscopic Characterization

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NMR spectra were recorded on JEOL ECZ600 spectrometers with deuterated solvents, the chemical shifts of which were used as an internal standard. Lowresolution electrospray ionization mass spectra (ESIMS) were obtained on a Shimadzu LCMS-2020 spectrometer. High-resolution electrospray ionization mass spectra (HRESIMS) were recorded on an AccuTOF-T100LP (JEOL) mass spectrometer. IR spectra were measured on ATR (attenuated total reflection) on a JASCO FT-IR 230 spectrophotometer. UV spectra were measured on a Shimadzu UV mini-1240 spectrometer.

Y.i.x.i.z.h.u.o.m.a., Ishikawa N., Abdelfattah M.S, & Ishibashi M. (2017). Elmenols C-H, new angucycline derivatives isolated from a culture of Streptomyces sp. IFM 11490. The Journal of antibiotics, 70(5).

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