The largest database of trusted experimental protocols

5 protocols using ammonium hydroxide solution

1

Electrochemical Material Synthesis Protocols

Check if the same lab product or an alternative is used in the 5 most similar protocols
The following chemicals were used for material
preparation and electrochemical analysis: graphite (Timrex KS44; Imreys,
Bodio, Switzerland), carbon black (Vulcan carbon XC72R; Cabot Corp.,
Boston, Massachusetts), hydrazine hydrate (reagent grade; Sigma-Aldrich,
Darmstadt, Germany), cobalt(II) nitrate hexahydrate (99.999% trace
metals basis; Sigma-Aldrich, Darmstadt, Germany), zinc(II) nitrate
hexahydrate (>99%; Honeywell Fluka, Charlotte, North Carolina),
cerium(III)
nitrate hexahydrate (99.5%; Alfa Aesar, Haverhill, Massachusetts),
manganese(II) nitrate tetrahydrate (98%; Alfa Aesar, Haverhill, Massachusetts),
ammonium hydroxide solution (30–33%; Honeywell, Charlotte,
North Carolina), 2-propanol (≥99.9%, UV/IR-grade; Carl Roth,
Karlsruhe, Germany), potassium hydroxide (1.0 M Fixanal 1 L Ampoule;
Merck, Darmstadt, Germany), ethanol (99.9% p.a.; Carl Roth, Karlsruhe,
Germany), Nafion solution (5 wt % in water; Quintech, Göppingen,
Germany), alumina suspension (0.05 μm; MasterPrep Bühler,
Lake Bluff, Illinois), and Pt/C (30 wt % on Vulcan; De Nora North
America, New Jersey). Ultrapure water (∼18 MΩ cm) was
used in all experiments.
+ Open protocol
+ Expand
2

Graphene Oxide Synthesis from Graphite

Check if the same lab product or an alternative is used in the 5 most similar protocols
Graphite (Timrex KS44), as the precursor for graphene oxide (GO) synthesis, was obtained from Imerys and carbon black (Vulcan XC72R) from Cabot Corp. was used. Hydrazine hydrate (N2H4·H2O, reagent grade), potassium hydroxide (KOH, 1.0 M Fixanal 1 L Ampoule) and cobalt(ii) nitrate hexahydrate (Co(NO3)2·6H2O, 99.999% trace metals basis) were supplied by Sigma Aldrich. Cerium(iii) nitrate hexahydrate (Ce(NO3)3·6H2O, 99.5%) and manganese(ii) nitrate tetrahydrate (Mn(NO3)2·4H2O, 98%) were delivered by Alfa Aesar. Ammonium hydroxide solution (30–33% NH3 in H2O) from Honeywell was used. Isopropyl alcohol (2-propanol, ≥99.9%, UV/IR-grade) and ethanol (EtOH, 99.9% p.a.) were purchased from Carl Roth. Nafion® solution (5 wt% in H2O) and a commercial carbon black supported platinum catalyst (Pt/C, 20 wt% on Vulcan) were supplied by Quintech. An alumina suspension (Al2O3, 0.05 μm particle size) from MasterPrep® Bühler served as RDE polishing agent. The ultrapure water used throughout all experiments was purified with a Barnstead NANOpureWater Purification system to the desired resistivity of approx. 18 MΩ cm.
+ Open protocol
+ Expand
3

Synthesis of Silica-PVP Nanocomposites

Check if the same lab product or an alternative is used in the 5 most similar protocols
Poly (vinyl pyrrolidone) (PVP) (MW: 1,300,000 g mol−1) and tetraethyl orthosilicate (TEOS) reagents were purchased from Sigma Aldrich. Ammonium hydroxide solution (30–33% NH3 in H2O) and ethanol (99.8% ACS) were purchased from Honeywell.
+ Open protocol
+ Expand
4

Analytical Standards for Food Analysis

Check if the same lab product or an alternative is used in the 5 most similar protocols
Folin−Ciocalteu reagent was purchased from Kemika (Zagreb, Croatia); 2,2-diphenyl-1-picrylhydrazyl, catechin (CAS: 154–23–4, ≥99.0%), epicatechin (CAS: 490–46–0; ≥98%), gallic acid (CAS: 149–91–7, ≥97.5), p-cumaric acid (CAS: 501–98–4, ≥98.0%), phloretin (CAS: 60–82–2, ≥99.0%), phloridzin (CAS: 60–81–1, ≥98%), chlorogenic acid (CAS: 327–97–9, ≥95%) and caffeic acid (CAS: 331–39–5, ≥98.0%) were obtained from Sigma Chemical Co. (St. Louis, MO, USA). Methanol (HPLC grade) and orthophosphoric acid (85%) were obtained from Panareac (Barcelona, Spain). Certified standard of patulin and MycoSep® 228 AflaPat columns were obtained from Romer Labs Biopure (Romer Labs, Tulln, Austria). Certified pesticide standard solutions were obtained from CPAchem (CPAchem, Stara Zagora, Bulgaria). LC-MS and HPLC grade acetonitrile was purchased from J.T. Baker (J.T. Baker, Deventer, The Netherlands), while LC-MS grade formic acid and LC-MS ammonium formate were produced by Sigma–Aldrich (Sigma-Aldrich, St. Louis, MO, USA). Ammonium hydroxide solution, ≥25% NH3 in H2O, was purchased from Honeywell (Offenbach, Germany). Nylon syringe filters, 0.2 µm pore size and 13 mm diameter, were obtained from Agilent (Santa Clara, CA, USA). Ultrapure water was generated by Niro VV system (Nirosta d.o.o., Osijek, Croatia).
+ Open protocol
+ Expand
5

Quantification of Periodontal Drug Release

Check if the same lab product or an alternative is used in the 5 most similar protocols
Atridox (doxycycline hyclate, 10%) was manufactured by Tolmar, Inc. (Fort Collins, CO). Arestin (minocycline HCl, 1 mg) was manufactured by Valeant Pharmaceuticals (Bridgewater, NJ). PerioChip (Chlorhexidine gluconate, 2.5 mg) was manufactured by Drexel Pharma Technologies Ltd (Yokneam, Israel). These periodontal drug products were purchased from their respective vendors via a dental clinic. Doxycycline hyclate USP and minocycline HCl USP were purchased from PCCA (Houston, TX). Chlorhexidine was purchased from Sigma-Aldrich (St. Louis, MO). Ammonium hydroxide solution (30%–33%) was purchased from Honeywell (Muskegon, MI). Triethylamine and trypsin (from porcine pancreas, lyophilized powder, 1,000–2,000 BAEE units/mg solid) were purchased from Sigma-Aldrich (St. Louis, MO). Sodium phosphate monobasic was from Acros Organics (Janssen Pharmaceuticalaan, Geel, Belgium). Tetrabutylammonium hydrogen sulfate was from TCI America (Portland, OR). Sodium chloride, potassium phosphate monobasic, ethylene diamine tetraacetic acid, and o-phosphoric acid were purchased from Fisher Scientific (Fair Lawn, NJ). Acetonitrile (HPLC grade) was from Pharmaco-AAPER (Shelbyville, KY). Materials were used as received.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!