All NMR spectra were recorded on a Bruker 600 MHz Avance II+ at 298 K equipped with a Prodigy TCI probe. One-dimensional 1H-NMR spectra were acquired with excitation sculpting for solvent suppression (Bruker pulse program: zgesgp), recording 512 scans.Two-dimensional 1H-13C-HSQC NMR spectra were recorded using a phase-sensitive ge-2D HSQC with water flip-back pulses and PEP with gradients in back-INEPT (Bruker pulse program hsqcetfpgpsi2): number of scans 72, spectral width in proton dimension 10 ppm, spectral width in carbon dimension 20 ppm, 2048×32 complex data points, 1J(1H,13C) = 200 Hz, interscan delay 1.0 s yielding an acquisition time of approx. 30 minutes per HSQC spectrum.
Hsqcetfpgpsi2
Manufactured by Bruker
The Hsqcetfpgpsi2 is a laboratory equipment product manufactured by Bruker. It is designed to perform heteronuclear single quantum coherence (HSQC) experiments, a commonly used nuclear magnetic resonance (NMR) technique for structural elucidation and analysis of chemical compounds.
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2 protocols using hsqcetfpgpsi2
1
NMR Spectroscopy of Organic Compounds
2
NMR Spectroscopy of Organic Compounds
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All NMR spectra were recorded on a Bruker 600 MHz Avance II+ at 298 K equipped with a Prodigy TCI probe. One-dimensional 1H-NMR spectra were acquired with excitation sculpting for solvent suppression (Bruker pulse program: zgesgp), recording 512 scans.Two-dimensional 1H-13C-HSQC NMR spectra were recorded using a phase-sensitive ge-2D HSQC with water flip-back pulses and PEP with gradients in back-INEPT (Bruker pulse program hsqcetfpgpsi2): number of scans 72, spectral width in proton dimension 10 ppm, spectral width in carbon dimension 20 ppm, 2048×32 complex data points, 1J(1H,13C) = 200 Hz, interscan delay 1.0 s yielding an acquisition time of approx. 30 minutes per HSQC spectrum.
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