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2 protocols using divinylbenzene

1

Synthesis of Magnetic Nanocomposites for Environmental Remediation

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Standard Formic acid (FA), mefenamic acid (MA), chloroamphenicol (CP), ketoprofen (KEP), clofibric acid (CA), indometacin (IDM), acetylsalicylic acid (ASP), bisphenol A (BPA), 2-phenylphenol, gemfibrozil (GEM), triclosan (TCS), and ibuprofen (IBU) (>98% of purity for all the chemicals) were purchased from J&K Scientific (Shanghai, China). Methanol (Tedia, USA) and acetonitrile (ACN) (Tedia, USA) were HPLC-grade. Divinylbenzene (DVB, 80%), benzoyl peroxide (BPO, 98%), toluene (TOL, 99.5%), oleic acid (OA), and 1,2-dichloroethane (DCE, 99%) were provided by Sinopharm Chemical Reagent Co., Ltd. (China). Ferric chloride hexahydrate (FeCl3 • 6H2O), ferrous chloride tetrahydrate (FeCl2 • 4H2O), anhydrous ferric chloride (FeCl3), N,N-dimethyl-1,3-propanediamine, ammonium hydroxide, and other inorganic salts (analytical grade) were purchased from Nanjing Chemical Reagent Co., Ltd. (Nanjing, China). Ultrapure water prepared by the Milli-Q water purification system (Billerica, MA, USA) was used for all experiments.
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2

Preparation of Magnetically-Responsive Polymer Sorbents

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λ-Cyhalothrin (LC), fenvalerate (FL) were supplied by Jiangsu Huangma Agrochemicals Co., Ltd. Fe3O4 nanoparticles (mean diameter is 250 nm), styrene (St), divinylbenzene (DVB), acrylamide (AM), oleic acid (OA), methacrylic acid (MAA), α,α′-azoisobutyronitrile (AIBN), toluene, methanol, acetone, chloroform, diethyl phthalate (DEP), and calcium chloride dihydrate (CaCl2·2H2O) were purchased from Sinopharm Chemical Reagent Co., Ltd (Shanghai, China). Hypermer 2,296 was purchased from CRODA UK. All chemicals were of analytical reagent grade. Water was freshly deionized and distilled.
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