4 chloronitrobenzene

Manufactured by Merck Group

Sourced in Germany

4-chloronitrobenzene is a chemical compound used as an intermediate in the production of various pharmaceutical and agrochemical products. It is a solid, crystalline substance that is typically yellow or orange in color. The primary function of 4-chloronitrobenzene is to serve as a precursor for the synthesis of other chemical compounds, rather than being an end-use product itself.

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2 protocols using 4 chloronitrobenzene

Synthesis and Characterization of Hybrid Microgels

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Styrene (STY), N-isopropylmethacrylamide (NIPM) (98%), N,N-methylenebisacrylamide (MBIS) (99%), ammonium per sulfate (APs) (99%), sodium dodecyl sulfate (SDS) (98%), sodium borohydride (NaBH₄) (98%), 2-nitrophenol (2NP), 4-nitrophenol (4NP), 3-nitrophenol (3NP), 4-chloronitrobenzene (4NCB), 2-nitroaniline (2NA), 3-nitroaniline (3NA), 4-nitroaniline (4NA), 2-amino-4-nitroanisole (2A4NA), 4-nitrophenylhydrazine (4NPH), 2,4-dinitrophenylhydrazine (2,4DNPH), and tetrachloroauric(iii) acid trihydrate (HAuCl₄·3H₂O) were obtained from Sigma Aldrich (Germany). No further purification of the chemicals was done except STY. STY was purified via vacuum filtration by passing it through alumina (Al₂O₃) to remove the inhibitor. Deionized water was used in all the experimental work. The membrane for dialysis (cut off = 12 000–14 000) was obtained from Scharlu and was used for the removal of unreacted reactants from the microgel and hybrid microgel dispersions.

Arif M., Shahid M., Irfan A., Nisar J., Wu W., Farooqi Z.H, & Begum R. (2022). Polymer microgels for the stabilization of gold nanoparticles and their application in the catalytic reduction of nitroarenes in aqueous media. RSC Advances, 12(9), 5105-5117.

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Chemical Synthesis of Nitro, Azo, and Halogenated Compounds

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Materials Nitrobenzene (99%), nitrosobenzene (97%), azoxybenzene, azobenzene (98%), hydrazobenzene, phenylhydroxylamine (97%), 4-chloroNitrobenzene (99%), 4chloroaniline (98%), 4-chlorobenzaldehyde (97%), 4-chlorobenzylalcohol (99%), 4-iodoNitrobenzene (98%), 4-iodoaniline (98%), 4-iodotoluene (99%), methanol (99.9%) and 1-butanol (99.7%) were all obtained from Sigma Aldrich. Potassium permanganate ($99%) was obtained from Fluka as was maleic acid ($98%). Metal precursors used were platinum nitrate (assay 15.14%) supplied by Johnson Matthey and palladium(II)nitrate hydrate procured from Sigma Aldrich. Research grade hydrogen was supplied by BOC. All chemicals were used as supplied.

McManus I.J., Daly H., Manyar H.G., Taylor S.F.R., Thompson J.M, & Hardacre C. (2016). Selective hydrogenation of halogenated arenes using porous manganese oxide (OMS-2) and platinum supported OMS-2 catalysts. Faraday discussions, 188.

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