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Ammonium molybdate tetrahydrate

Manufactured by Thermo Fisher Scientific

Ammonium molybdate tetrahydrate is a chemical compound with the molecular formula (NH4)6Mo7O24·4H2O. It is a yellowish-white crystalline solid that is soluble in water. The compound is commonly used as a reagent in analytical chemistry and biochemistry applications.

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2 protocols using ammonium molybdate tetrahydrate

1

Synthesis of Platinum-Based Electrocatalyst

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Ammonium molybdate tetrahydrate (AMT, (NH4)6Mo7O24·4H2O, 99%) was obtained from Alfa Aesar. Aniline (C6H7N, 99.5%), phytic acid (PA, C6H18O24P6, 90%), ammonium persulfate (APS, (NH4)2S2O8, 98%), and hydrochloric acid (HCl, 36–38%) were purchased from Shanghai Lingfeng Chemical Reagent, Shanghai Macklin Biochemical, Aladdin Industrial Corporation and Shanghai Titan Scientific Co., LTD, respectively. The commercial Pt/C (20 wt%) catalyst was obtained from Johnson Matthey. All the reagents were used as received without further treatment.
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2

Synthesis of Metal-Nitrogen-Carbon Single-Atom Catalysts

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In total, 60 mg of PC, 0.3 mmol of iron (III) nitrate nonahydrate (Alfa Aesar Co., Ltd.), and 6.7 mmol of α-D-glucose (Sinopharm Chemical Reagent Co., Ltd.) were dispersed in 5 mL of ultrapure water, and sonicated for 30 min to get a homogenous black suspension. The slurries were harvested after washing with water and drying at 60 °C, and then grounded together with melamine (Alfa Aesar Co., Ltd.) at a mass ratio of 1:5. The obtained powder was placed into a tube furnace and heated to 800 °C under Ar flow (100 sccm). After 2 h of pyrolysis, the black Fe–NC SAC was obtained. M–NC SACs (M = Mn, Co, Ni, Cu, Mo, and Pt) were prepared via the same procedures, except for using manganese nitrate hexahydrate (Alfa Aesar Co., Ltd.), cobalt nitrate hexahydrate (Alfa Aesar Co., Ltd.), nickel nitrate hexahydrate (Alfa Aesar Co., Ltd.), cupric nitrate hemipentahydrate (Alfa Aesar Co., Ltd.), ammonium molybdate tetrahydrate (Alfa Aesar Co., Ltd.), and (hydro)chloroplatinic acid (Alfa Aesar Co., Ltd.) as the metal precursor, respectively.
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