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Tc 125mt

Manufactured by Mettler Toledo

The TC-125MT is a thermal conductivity meter designed for measuring the thermal conductivity of materials. It provides accurate and reliable measurements of thermal conductivity, a key property in various industrial and research applications.

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Lab products found in correlation

2 protocols using tc 125mt

1

Thermal Transition Characterization of Materials

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The material’s
thermal transitions and melting/fusion enthalpies were measured using
a Mettler Toledo DSC2 calorimeter equipped with an HSS7 sensor and
a TC-125MT intercooler. The endotherms were recorded when the temperature
was raised from 25 to 160 °C, cooled back to −50 °C,
and reheated to 150 °C, at a rate of 10 °C min–1 with a nitrogen flow of 60 mL min–1. The crystallization
temperature (Tc) from the cooling scan
and melting temperature (Tm) from the
melting temperature during the second heating scan were taken as the
peak value of the crystallization or melting enthalpy in triplicate
measurements.
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2

Polymer Crystallization Kinetics Analysis

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Isotherms were
recorded under nitrogen using a heat-flux differential scanning calorimeter
(DSC) from Mettler Toledo (DSC2) equipped with a high-sensitivity
sensor (HSS9+) and a TC-125MT intracooler. Mettler 20 μL Al
crucible light sample pans were used; the sample weight was around
6 mg. Samples were first molten at 130 °C, which is significantly
above Tm in order to remove seed crystals,
for 30 min followed by rapid cooling at rate of −100 °C/min
to the desired isothermal crystallization temperature between 20 to
75 °C, where isotherms were recorded over the course of up to
30 000 s. A data point was taken every 3 s. The original data
was smoothed with a Savitzky–Golay method where the window
size was set to be 200 data points. After that, a baseline was subtracted
(the data processing is demonstrated in Figure S2). Origin 8 was used to fit processed data with a 3-parameter
Avrami eq (eq 2).
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