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Xrd 6000 powder

Manufactured by Shimadzu

The Shimadzu XRD-6000 is an X-ray diffractometer designed for powder sample analysis. It is capable of identifying crystalline phases and determining the structural properties of materials. The XRD-6000 utilizes a high-intensity X-ray source and a precision goniometer to accurately measure the diffraction patterns of powder samples.

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2 protocols using xrd 6000 powder

1

Structural and Magnetic Characterization

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The phases of the obtained samples were characterized by X-ray diffraction (XRD) on a Shimadzu XRD-6000 powder X-ray diffractometer with Cu Kα radiation (λ = 1.5418 Å). The morphologies of the samples were investigated on a Hitachi S-4800 field-emission scanning electron microscope (FE-SEM) at an acceleration voltage of 10.0 KV. Transmission electron microscopy (TEM), high-resolution TEM (HRTEM) images and the corresponding selected area electron diffraction (SAED) were obtained on the JEOL JEM-2100 transmission electron microscope at an acceleration voltage of 200 KV. The magnetic measurements were carried out using a SQUID magnetometer (Quantum Design) at 300 K.
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2

Powder X-Ray Diffraction Analysis

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The XRD measurements were carried out using a Shimadzu XRD-6000 powder X-ray diffraction unit with Cu Kα at 30 mA and 30 kV, in the 2θ range of 5° to 90°.
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