All chemicals were purchased from commercial companies and used without further purification. Elemental analyses (CHN) were carried out on Thermo-Finnigan Flash EA1112. IR spectra were recorded on a Shimadzu FT-IR 8300 infrared spectrophotometer. Electronic spectra were recorded on a Shimadzu UV-1280. The 1H (250 MHz) spectra were recorded on a Bruker Advance DPX 250 MHz spectrometer in CDCl3 solvent, using tetramethylsilane (TMS) as an internal standard. X-ray single-crystal diffraction experiment was performed on an Oxford Sapphire CCD diffractometer. The progress of the reactions was monitored by TLC using silica gel Polygram's SIL G/UV 254 plates. All reaction yields refer to the isolated products.
Ft ir 8300 infrared spectrophotometer
Manufactured by Shimadzu
The Shimadzu FT-IR 8300 is an infrared spectrophotometer that uses Fourier Transform Infrared (FT-IR) technology to analyze the absorption and transmission characteristics of a sample. It is capable of detecting and identifying various chemical compounds and functional groups within a sample.
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Lab products found in correlation
2 protocols using ft ir 8300 infrared spectrophotometer
1
Spectroscopic Characterization of Novel Compounds
2
Synthesis and Characterization of Metal Complexes
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All the chemicals and solvents were of analytical reagent grade quality. Benzoylacetone, acetylacetone, 1,1,1-trifluoro-2,4-pentanedione, 1,2-ethylenediamine, 1,2-diaminopropane, 1,3-diaminopropane, ammonia solution, carbon disulfide, dimethylsulfate, cyclopentanone, methanol, ethanol, chloroform, dimethylformamide, hydrochloric acid and dimethyltindichloride were purchased from Merck, Fluka and Aldrich chemical companies and were used as received without further purification.
The melting points of the compounds were determined by a melting point apparatus SMP1 stuart scientific. The IR spectra were recorded by Shimadzu FTIR 8300 infrared spectrophotometer in the range of 400-4000 cm -1 as KBr discs. Mass spectra were obtained on Perkin Elmer R MU-6E instrument. Elemental analyses (CHNS) were performed on a Termo Fininngan-Flash-1200 elemental analyzer. The molar conductance of ca. 10 -3 M solutions at 25±1 °C of the complexes in DMF were measured by means of a Jenway 4310 conductivity meter and a diptype cell with a platinized electrode. 1 H NMR spectra were acquired on Bruker Avance DPX 250 MHz instruments.
The melting points of the compounds were determined by a melting point apparatus SMP1 stuart scientific. The IR spectra were recorded by Shimadzu FTIR 8300 infrared spectrophotometer in the range of 400-4000 cm -1 as KBr discs. Mass spectra were obtained on Perkin Elmer R MU-6E instrument. Elemental analyses (CHNS) were performed on a Termo Fininngan-Flash-1200 elemental analyzer. The molar conductance of ca. 10 -3 M solutions at 25±1 °C of the complexes in DMF were measured by means of a Jenway 4310 conductivity meter and a diptype cell with a platinized electrode. 1 H NMR spectra were acquired on Bruker Avance DPX 250 MHz instruments.
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