Chloroplatinic acid hydrate (iv ) (H2PtCl6·xH2O, 99.99%), palladium(ii ) acetylacetonate (Pd(acac)2, 99%), copper(ii ) acetylacetonate (Cu(acac)2, 99%), trioctylphosphine oxide (TOPO, AR) were purchased from Sigma-Aldrich. Oleylamine (OAm, 80–90%) was purchased from Aladdin. Commercial Pt/C (20 wt%) were purchased from Alfa Aesar. Benzyl alcohol (BA), dimethylformamide (DMF), ethanol, acetone, chloroform and toluene were purchased from Sinopharm Chemical Reagent. All the chemicals and materials were used as received.
Palladium 2 acetylacetonate
Manufactured by Merck Group
Sourced in United States
Palladium(II) acetylacetonate is an organometallic compound with the chemical formula Pd(acac)2. It is a yellow crystalline solid that is used as a precursor in the synthesis of other palladium-containing compounds and materials. The compound contains a central palladium atom coordinated to two acetylacetonate ligands.
Automatically generated - may contain errors
Lab products found in correlation
Oleylamine, by Merck Group (6 mentions)
Acetone, by Sinopharm (3 mentions)
Chloroform, by Sinopharm (3 mentions)
Copper 2 acetylacetonate, by Merck Group (3 mentions)
Platinum 2 acetylacetonate, by Merck Group (3 mentions)
Oleic acid, by Merck Group (3 mentions)
Toluene, by Sinopharm (2 mentions)
Polyvinylpyrrolidone, by Merck Group (2 mentions)
Toluene, by Beijing Chemical Works (2 mentions)
Ethanol, by Beijing Chemical Works (2 mentions)
Methanol, by Beijing Chemical Works (2 mentions)
Perchloric acid solution, by Beijing Chemical Works (2 mentions)
Silver nitrate, by Merck Group (2 mentions)
Nafion 117 solution, by Merck Group (2 mentions)
Tungsten hexacarbonyl, by Merck Group (2 mentions)
Benzyl ether, by Merck Group (2 mentions)
1 2 hexadecanediol, by Merck Group (2 mentions)
Toluene, by Carlo Erba (1 mentions)
Octadecene, by Merck Group (1 mentions)
Copper chloride, by Merck Group (1 mentions)
11 protocols using palladium 2 acetylacetonate
1
Synthesis of Pt-based Nanoparticle Catalysts
2
Synthesis of Copper-Palladium Nanocomposites
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Copper
chloride (CuCl, anhydrous, 99.99%),
palladium(II) acetylacetonate [Pd(ac)2, 99%], ascorbic
acid (AA), oleylamine (OM, >70%), and octadecene (ODE, 90%) were
purchased
from Sigma-Aldrich. Elemental sulfur (99%) was from Strem Chemicals,
and ethanol (anhydrous, 99.9%), methanol (anhydrous, 99.9%), and toluene
(anhydrous, 99.8%) were from Carlo Erba reagents. All chemicals were
used as received without further purification.
chloride (CuCl, anhydrous, 99.99%),
palladium(II) acetylacetonate [Pd(ac)2, 99%], ascorbic
acid (AA), oleylamine (OM, >70%), and octadecene (ODE, 90%) were
purchased
from Sigma-Aldrich. Elemental sulfur (99%) was from Strem Chemicals,
and ethanol (anhydrous, 99.9%), methanol (anhydrous, 99.9%), and toluene
(anhydrous, 99.8%) were from Carlo Erba reagents. All chemicals were
used as received without further purification.
3
Synthesis of Pt-based Nanoparticle Catalysts
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Palladium(ii ) acetylacetonate (Pd(acac)2, 99%), copper(ii ) acetylacetonate (Cu(acac)2), poly(vinylpyrrolidone) (PVP, MW = 29 000), chloroplatinic(iv ) acid (H2PtCl6, 99.9%) were all purchased from Sigma Aldrich. Commercial Pt/C (20 wt%) were purchased from Alfa Aesar. Oleylamine (OAm, 80–90%) was purchased from Aladdin. Benzyl alcohol (BA), dimethylformamide (DMF), ethanol, acetone, chloroform and toluene were purchased from Sinopharm Chemical Reagent. All the chemicals and materials were used as received. All aqueous solutions were prepared using ultrapure water with a resistivity of 18.2 MΩ cm.
4
Synthesis of Metallic Nanoparticles
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Silver nitrate (AgNO3, ACS reagent, ≥99.0%), palladium(II) acetylacetonate (Pd(acac)2, 99%), gold(III) chloride trihydrate (HAuCl4·3H2O, ACS reagent, ≥49.0% Au basis), oleylamine (70%, technical grade) and Nafion 117 solution (5% in a mixture of lower aliphatic alcohols and water) were purchased from Sigma-Aldrich. Ethanol (>99.7%), mEthanol (>99%), toluene (>99.5%) and perchloric acid solution (70%) were purchased from Beijing Chemical Works. Vulcan XC-72 carbon powders (XC-72C with BET surface area of 250 m2 g−1 and average particle size of 40 ∼ 50 nm) were purchased from Cabot. Commercial Pd/C catalyst was purchased from Johnson Matthey (JM). All chemicals were used as received. Deionized water was distilled by a Milli-Q Ultrapure-water purification system. All glassware and Teflon-coated magnetic stirring bars were cleaned with aqua regia, followed by copious rinsing with deionized water before drying in an oven.
5
Catalytic Conversion of Levulinic Esters
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Methyl levulinate (≥99%), n-octanol (≥99%), n-decanol (≥98%), n-dodecanol (≥98%), n-hexadecanol (≥99%), n-octadecanol (≥96%), 2-pentanone (≥98%), cyclopentanone (≥99%), 2-heptanone (≥98%), pivaldehyde (≥96%), 2ethylhexanal (≥96%), 2-decyl-1-tetradecanol (≥97%), Palladium (II) acetylacetonate (≥99%) and commercial 5%Pd/C, were purchased from Sigma-Aldrich. Carbon NORIT® RX 3 extra was purchased from NORIT.
6
Synthesis of Colloidal Nanocrystals
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Palladium(II) acetylacetonate
(97%), copper(II)
acetylacetonate (97%), benzyl ether (99.8%), 1,2-hexadecanediol (90%),
oleic acid (OlAc, 90%), oleylamine (OlAm, 70%), platinum(II) acetylacetonate
(98%), 1-octadecene (ODE, 90%), borane morpholine complex (MB, 95%),
tertbutylamine-borane complex (TBAB, 97%), copper(I) acetate (97%),
trioctylamine (98%), and solvents (anhydrous chloroform, anhydrous
isopropanol, toluene, and hexane) needed to synthesize the NCs were
purchased from Sigma-Aldrich and used as received without further
purification. γ-Al2O3 powder (extrudate
from Sigma-Aldrich, crushed and sieved to 90 μm mean size, BET
specific surface area 190 m2 g–1) was
purchased from Strem Chemicals.
(97%), copper(II)
acetylacetonate (97%), benzyl ether (99.8%), 1,2-hexadecanediol (90%),
oleic acid (OlAc, 90%), oleylamine (OlAm, 70%), platinum(II) acetylacetonate
(98%), 1-octadecene (ODE, 90%), borane morpholine complex (MB, 95%),
tertbutylamine-borane complex (TBAB, 97%), copper(I) acetate (97%),
trioctylamine (98%), and solvents (anhydrous chloroform, anhydrous
isopropanol, toluene, and hexane) needed to synthesize the NCs were
purchased from Sigma-Aldrich and used as received without further
purification. γ-Al2O3 powder (extrudate
from Sigma-Aldrich, crushed and sieved to 90 μm mean size, BET
specific surface area 190 m2 g–1) was
purchased from Strem Chemicals.
7
Synthesis of Metal Acetylacetonates
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Palladium(II) acetylacetonate [Pd(acac)2, 99%], platinum(II) acetylacetonate [Pt(acac)2, 97%], nickel(II) acetylacetonate [Ni(acac)2, 95%], rhodium(III) acetylacetonate [Rh(acac)3, 97%], copper(II) acetylacetonate [Cu(acac)2, 99.9%], poly(vinylpyrrolidone) (PVP, MW≈29000), oxalic acid (OA), hexadecyltrimethylammonium bromide (CTAB), oleylamine (OAm), and tungsten hexacarbonyl [W(CO)6] were all purchased from Sigma Aldrich. Commercial Pt black and Pt/C (20 wt%) were purchased from Alfa Aesar. Benzaldehyde (BAL), benzyl alcohol (BA), dimethylformamide (DMF), ethanol, acetone, chloroform, and toluene were purchased from Sinopharm Chemical Reagent. All syntheses were carried out in a glass flask (25 mL, Shuniu) or home-made 15 mL Teflon-lined stainless-steel autoclave. Deionized water (18.2 MΩ/cm) was used in all experiments. All the chemicals were used as received without further purification.
8
Synthesis of Pt/Pd Catalysts on Vulcan Carbon
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Silver nitrate (AgNO3, ACS reagent, ≥99.0%), platinum(II) acetylacetonate (Pt(acac)2, 97%), palladium(II) acetylacetonate (Pd(acac)2, 99%), oleylamine (70%, technical grade) and Nafion 117 solution (5% in a mixture of lower aliphatic alcohols and water) were purchased from Sigma-Aldrich. Ethanol (>99.7%), mEthanol (>99%), toluene (>99.5%), perchloric acid solution (70%), sodium chloride (NaCl, analytical grade) and acetic acid (C2H4O2, analytical grade) were purchased from Beijing Chemical Works. Vulcan XC-72 carbon powders (XC-72C with BET surface area of 250 m2 g−1 and average particle size of 40 ∼ 50 nm) were purchased from Cabot. All chemicals were used as received. Deionized water was distilled by a Milli-Q Ultrapure-water purification system. All glassware and Teflon-coated magnetic stirring bars were cleaned with aqua regia, followed by copious rinsing with deionized water before drying in an oven.
9
Synthesis of Bimetallic Nanoparticle Catalysts
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Palladium(II) acetylacetonate (Pd(acac)2, 99%), rhodium(III) acetylacetonate (Rh(acac)3, 97 %), silver acetate (C2H3AgO2, 99%), hexadecyl trimethyl ammonium bromide (CTAB, 99%), tungsten hexacarbonyl (W(CO)6, 97%), oleylamine (C18H37N, OAm, > 70%), oleic acid (C18H34O2, OA, > 85%) and Nafion (5%) were all purchased from Sigma-Aldrich. Commercial Pt (20 wt % Pt nanoparticles with an average size of 2∼3 nm on Vulcan XC-72 carbon) was purchased from Johnson Matthey Corporation. Glucose (C6H12O6•H2O, analytical reagent), potassium hydroxide (KOH, analytical reagent, ≥ 85%), cyclohexane (C6H12, analytical reagent, ≥ 99.5%), methanol (CH4O, analytical reagent, ≥ 99.7%), ethanol (C2H6O, analytical reagent, ≥ 99.7%) and isopropanol (C3H8O, analytical reagent, ≥ 99.7%) were obtained from Beijing Tongguang Fine Chemicals Company. All the chemicals were used as received without further purification. The water (18 MΩ/cm) used in all experiments was prepared by passing through an ultra-pure purification system.
10
Synthesis of Metallic Nanoparticles
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Platinum(II) acetylacetonate (97%), palladium(II) acetylacetonate (99%), copper(II) acetylacetonate (98%), benzyl ether (99%), oleylamine (70%), oleic acid (99%), and 1,2-hexadecanediol (90%) were purchased from Aldrich. Other chemicals used, such as ethanol and hexane, were purchased from Fisher Scientific. Vulcan carbon XC-72 was purchased from Cabot. Commercial Pt/C catalyst (E-tek 20 wt% loading) was obtained from Strem Chemicals. All chemicals were used as received. Gases such as N2, O2, and H2 were obtained from Airgas. Millipore Milli-Q water was used.
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