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Ethyl 4 dimethylamino benzoate edmab

Manufactured by Merck Group
Sourced in United States, China

Ethyl 4-dimethylamino-benzoate (EDMAB) is a chemical compound used as a photoinitiator in the manufacturing of various materials. Its core function is to facilitate the initiation of polymerization reactions upon exposure to light.

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8 protocols using ethyl 4 dimethylamino benzoate edmab

1

Synthesis and Characterization of Antibacterial Monomers

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The chemical structures of the different reactants are shown in Fig. 1. Bisphenol A glycerolate dimethacrylate (bis-GMA), tri(ethyleneglycol) dimethacrylate (TEGDMA), camphorquinone (CQ), and ethyl 4-dimethylamino-benzoate (EDMAB) were purchased from Sigma-Aldrich (St. Louis, MO, USA). QAS antibacterial monomers (MAE-DB and TMH-DB), with the molecular formula shown in Fig. 1, were supplied by Xylmed Biomedical (Xi'an, China). All materials were used as received without further purification.
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2

Synthesis and Characterization of Dentin Adhesives

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2,2-bis[4-(2-hydroxy-3-methacryloxypropoxy)phenyl]-propane (BisGMA, Polysciences, Warrington, PA) and 2-hydroxyethyl methacrylate (HEMA, Acros Organics, NJ) were used as received without further purification as monomers in dentin adhesives. 2-Aminoethyl methacrylate hydrochloride (AEMA) was used as a co-monomer as obtained from Sigma Aldrich (St. Louis, MO). Camphoroquinone (CQ) and ethyl-4-(dimethylamino)benzoate (EDMAB) were obtained from Sigma-Aldrich (St. Louis, MO). All other chemicals were reagent grade and used without further purification. MMP-8 colorimetric and fluorimetric RED kits were bought from Enzo life sciences and used as instructed. Peptides Asn-Cys-Cys (MAP), Ser-Trp-Leu-Ala-Tyr-Pro-Gly-Ala-Val-Ser-Tyr-Arg-Gly-Asn-Cys-Cys (tether-MAP), and Disuccinimidyl suberate (DSS) linker were gifts from Echogen Inc.
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3

Polymeric Membranes for Water Treatment

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Unless or else stated, all the reagents and chemicals are of analytical grades. For the preparation of substrate membrane, materials and synthesis processes are adopted from our previous work14 (link). For the active layer preparation, methacrylic acid (MAA) (SRL Chem, India, Mw. 86.09), poly(ethylene glycol) phenyl ether acrylate (PPEA) (Sigma-Aldrich, Mw. 324) as monomer, camphorquinone (CQ) as photo initiator and ethyl 4-dimethylaminobenzoate (EDMAB) as an accelerator are purchased from Sigma-Aldrich. For a control polyamide active layer preparation, trimesoyl chloride (TMC), m-phenylenediamine (MPD), and n-hexane were purchased from Sigma-Aldrich.
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4

Bioactive Polymer Composite Synthesis

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Poly(tetrahydrofuran ether glycol) 1000 (PTMEG 1000), 2-hydroxyethyl methacrylate (HEMA), triethylene glycol dimethacrylate (TEGDMA), dibutyltin dilaurate (DBTDL), acrylic acid (AA), isophorone diisocyanate (IPDI), 2,2-dihydroxymethylpropionic (DMPA), γ-methacryloxypropyl trimethoxy silane (γ-MTS), 2,2-dihydroxymethylpropionic, triethylenediamine, camphorquinone (CQ), ethyl-4-dimethylamino-benzoate (EDMAB), acetic acid and nHAp were purchased from Sigma Aldrich Corp, St. Louis (MO, USA). Tetrahydrofuran (THF) was supplied by Tianjin Tiantai Refine Chemicals Co., Ltd. (Tianjin, China). Peptide DDDEEKC was obtained from ChinaPeptide (Shanghai, China). Simulated body fluid (SBF) was obtained from Beijing Leagene Biotechnology Co., Ltd. (Beijing, China). Potassium hydroxide was supplied by Beijing Chemical Co. (Beijing, China).
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5

Synthesis and Characterization of Hybrid Biomaterial

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Ditin butyl dilaurate (DBTDL), 2-hydroxyethyl acrylate (HEA), 3-aminopropyltriethoxy silane (APS), and bromocresol green indicator (BCG) were obtained from Aladdin Industrial Corporation, Shanghai, China. Absolute ethanol was purchased from Hangzhou Gaojing Fine Chemical Co. Ltd., Hangzhou, China. Camphorquinone (CQ) and ethyl-4-dimethylaminobenzoate (EDMAB) were obtained from Sigma Aldrich, Shanghai, China. TiO2, Isophorone diisocyanate (IPDI) and polypropylene glycol (PPG) were purchased from Aladdin Industrial Corporation, Shanghai, China. Deionised water (>18 MΩ·cm, Millipore Milli-Q, Suzhou, China) was used for all experiments. All chemical reagents were of analytical grade, except BGC, which was of indicator grade, and were used without additional purification.
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6

Dental Composite Material Formulation

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The following reagents were used in the study: 2-hydroxyethylmethacrylate (HEMA, Sigma–Aldrich, St. Louis, MO, USA), bisphenol glycerolate dimethacrylate (BisGMA; Esstech, Essington, PA, USA), triethylene glycol dimethacrylate (TEGDMA, Esstech), photoinitiator campho9rquinone (CQ, Sigma-Aldrich), ethyl 4-(dimethylamino)benzoate (EDMAB, Sigma-Aldrich), and white PC (P. W. Grade 52.5) provided by the Aalborg Portland Group (Anqing, China). The QAS antibacterial monomer (MAE-DB) was developed by our team.
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7

Synthesis of Photopolymerizable POSS Composites

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The chemical structures of the different reactants are shown in Figure 1. Methacryl isobutyl POSS (MI-POSS) and methacryl POSS (MA-POSS) were purchased from Hybrid Plastics Company (Hattiesburg, MS, USA). Ethyl 4-dimethylaminobenzoate (EDMAB) and camphorquinone (CQ) were purchased from Sigma-Aldrich Company (St Louis, MO, USA). Bis-GMA, TEGDMA, and the 0.7 μm silinated barium borosilicate glass (V-117-4107) were provided by Esstech, Inc (Essington, PA, USA). All materials were used as received without further purification.
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8

Photopolymerizable Dental Composite Formulation

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Bisphenol A glycidyl dimethacrylate (BisGMA), 2 hydroxyethyl methacrylate (HEMA), Camphoroquinone (CQ), Ethyl-4(dimethylamino) benzoate (EDMAB), and Diphenyliodonium hexafluorophosphate (DPIHP), 2-isocyanatoethyl methacrylate, and 2-butanone were procured from Sigma Aldrich, Inc. St. Louis, MO, US. Sodium hydroxide (NaOH) and methacryloxypropyl (trimethoxy) silane were procured from Fischer Scientific and Gelest Inc., Waltham, MA, USA, respectively.
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