All solvents were purchased in the highest available quality required for their application in this study. The reactions requiring anhydrous conditions were carried out under argon atmosphere using anhydrous solvents treated with activated molecular sieves for at least 24 h. molecular sieves (4Å and 3Å) were purchased from Alfa Aesar (Karlsruhe, Germany) and heat-activated under vacuum before use. Triethylamine, trityl chloride, toluene-sulfonyl chloride, NaHCO3, Na2SO4, 1,4-butanediol, P2O5, sodium hydride, n-butyllithium (1.6 M solution in hexane), (3-bromopropoxy)-tert-butyldimethylsilane, (4 ) and ethylene oxide (2.9–3.1 M solution in THF) were purchased from Sigma Aldrich (Steinheim, Germany). Cobalt bis(1,2-dicarbollide) was purchased from Katchem Ltd., Prague, Czech Republic.
Toluene sulfonyl chloride
Manufactured by Merck Group
Sourced in Germany
Toluene-sulfonyl chloride is a chemical compound used as a reagent in organic synthesis. It is a colorless crystalline solid with the molecular formula C7H7ClSO2. Toluene-sulfonyl chloride is commonly used as a protecting group for alcohols and amines in various chemical reactions.
Automatically generated - may contain errors
Lab products found in correlation
Triethylamine, by Merck Group (2 mentions)
Sodium hydride, by Merck Group (1 mentions)
Ethylene oxide, by Merck Group (1 mentions)
Trityl chloride, by Merck Group (1 mentions)
Molecular sieves, by Thermo Fisher Scientific (1 mentions)
1 4 butanediol, by Merck Group (1 mentions)
N butyllithium, by Merck Group (1 mentions)
Nahco3, by Merck Group (1 mentions)
Na2so4, by Merck Group (1 mentions)
Ethylenediamine, by Merck Group (1 mentions)
2 protocols using toluene sulfonyl chloride
1
Synthetic Protocols for Complex Molecules
2
Hylon VII Biopolymer Modification
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Starch Hylon VII was donated
by Ingredion, Germany. Fresh human blood was donated by Central Institute
of Blood Transfusion in Innsbruck, Austria. The use of this human
biomaterial was approved by the local ethics committee (Medical University
of Innsbruck). Toluenesulfonyl chloride, triethylamine, ethylenediamine,
medium-molecular weight chitosan (75–85% deacetylated), 2,4,6-trinitrobenzene
sulfonic acid solution (TNBS), Triton X-100, and sterile Dulbecco’s
phosphate-buffered saline were purchased from Sigma-Aldrich, Germany.
All other components were of analytical grade and used without further
purification.
by Ingredion, Germany. Fresh human blood was donated by Central Institute
of Blood Transfusion in Innsbruck, Austria. The use of this human
biomaterial was approved by the local ethics committee (Medical University
of Innsbruck). Toluenesulfonyl chloride, triethylamine, ethylenediamine,
medium-molecular weight chitosan (75–85% deacetylated), 2,4,6-trinitrobenzene
sulfonic acid solution (TNBS), Triton X-100, and sterile Dulbecco’s
phosphate-buffered saline were purchased from Sigma-Aldrich, Germany.
All other components were of analytical grade and used without further
purification.
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