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6 protocols using sulphuric acid h2so4

1

Synthesis and Characterization of Silane-Modified Silver Nanoparticles

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3-Mercaptopropyl trimethoxysilane (MPTMS, 97%) was obtained from J&K Scientific Ltd. (Beijing, China). Allyltriethoxysilane (ATOS) was purchased from TCI Development Co. Ltd. (Shanghai, China). Silver nitrate (AgNO3, 99.8%), ammonium hydroxide (NH4OH, 28%), sulphuric acid (H2SO4, 98%), hydrogen peroxide (H2O2, 30%) were obtained from Sinopharm Chemical Reagent Co. Ltd. (Shanghai, China) Tryptic soy broth medium (TSB) and tryptic soy agar medium (TSA) were purchased from Hangzhou Microbial Reagent Co., Ltd. (Hangzhou, China) Fluorescent dyes Hoechst33342 and PI were purchased from Beijing Solarbio science & technology Co., Ltd.(Beijing, China) All the reagents were used without further purification.
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2

Graphite-LiFePO4 Battery Electrode Fabrication

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Graphite powders (100 mesh, Nanjin XFNANo), LiFePO4 cathode slurry (MTI Co.), Lithium bis(trifluoromethanesulfonyl) imide (LiTFSI, Alfa Aesar), Poly(ethylene oxide) (PEO, Mw=1000000, Sigma), 1-(3-aminopropyl)-3-methylimidazolium bromide (Lanzhou Institute of Chemical Physics), Potassium permanganate (KMnO4, Sinopharm), Sulphuric acid (H2SO4, concentrated, Sinopharm), Hydrogen peroxide (H2O2, Sinopharm), Potassium hydroxide (KOH, Sinopharm), Sodium nitrate (NaNO3, Sinopharm).
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3

Fabrication of Ag-Cr Nanocomposites

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Ag and chromium (Cr) pellets both with 99.99% purity were purchased from Jinyu Aochen (Beijing). The H2O2 solution, ethanol (C2H5OH) and sulphuric acid (H2SO4) were purchased from Sinopharm (Shanghai). Si wafers were used as the substrate. BPE was purchased from Sigma-Aldrich (USA). Milli-Q water (resistance rate of ≥18.2 MΩ cm) was produced using the Milli-Q system.
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4

Phytochemical Extraction and Characterization

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The GA3 (CAS# 77-06-5), NDGA (≥97%, CAS# 500-38-9) and Vanillin (CAS# 121-33-5) were purchased from Sigma-Aldrich (Shanghai) Trading Co., Ltd., Shanghai, China. KNO3 (CAS# 7757-79-1), H2O2 (30%, CAS# 7722-84-1), sulphuric acid (H2SO4, CAS 7664-93-9) and hydrochloric acid (HCl, CAS# 7647-01-0) were purchased from Sinopharm Chemical Reagent Co., Ltd., Shanghai, China. Sodium hypochlorite (NaClO, CAS# 7681-52-9) was bought from Sangon Biotech (Shanghai) Co., Ltd., Shanghai, China. A pure supply of PAs (UV ≥ 95%, CAS 4852-22-6) was purchased from Shanghai Aladdin Biochemical Technology Co., Ltd., Shanghai, China. Ethanol (99.7%, CAS# 64-17-5) and mEthanol (99.7%, CAS# 67-56-1) was purchased from Shanghai Titan Scientific Co., Ltd., Shanghai, China. Sodium hydroxide (NaOH, CAS# 1310-73-2) was purchased from Shanghai Chemical Reagent Co., Ltd., Shanghai, China. Murashige and Skoog (MS) medium was purchased from Qingdao Hope Bio-Technology Co., Ltd., Shandong, China. The GA3 and NDGA stock solutions (100 mM) were prepared by dissolving in 80% mEthanol. KNO3 stock solution (10%) was prepared by dissolving in distilled water. All stock solutions were diluted in distilled water to make working solutions.
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5

Synthesis and Characterization of Magnesium Silicate Photocatalysts

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The chemicals for preparing
MgSiPCs were obtained from Sinopharm Chemical Reagent Co., Ltd (China),
including magnesium sulfate (MgSO4), sodium silicate (Na2SiO3), sulphuric acid (H2SO4, purity ≥ 98 wt %), and sodium hydroxide (NaOH, purity ≥
96 wt %). Reactive yellow 2 (C25H15Cl3N9Na3O10S3) and reactive
blue 2 (C29H20ClN7Na3O11S3) were purchased from Hefei Meifeng Chemical
Reagent Co., Ltd (China). Distilled water was used to prepare the
aqueous solution throughout the study.
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6

Synthesis and Characterization of Ti3AlC2/CNF Composites

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All chemicals were used without further purification. Titanium aluminium carbide (Ti3AlC2, ~400 mesh, 98%) was purchased from Yiyi Technology Co., Ltd., Jilin, China, CNF suspension (0.55 wt%) from Hongqi Technology Co., Ltd., Guilin, China and sulphuric acid (H2SO4, 99.8%) from Sinopharm Chemical Reagent Co., Ltd., Shanghai, China). Lithium fluoride (LiF, 99.7%), ammonium persulfate ((NH4)2S2O8, 99.7%), aniline (C6H7N, 97.7%) and potassium hydroxide (KOH, 97.7%) were obtained from Sigma-Aldrich Co., Ltd., Shanghai China. Hydrochloric acid (HCl, 37%) and ethanol (C2H6O, 99%) were sourced from a local supplier.
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